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ChemicalBook--->CAS DataBase List--->22280-60-0

22280-60-0

22280-60-0 Structure

22280-60-0 Structure
IdentificationMore
[Name]

6-Chloro-2-methyl-3-nitropyridine
[CAS]

22280-60-0
[Synonyms]

2-CHLORO-3-NITRO-6-METHYL PYRIDINE
2-CHLORO-3-NITRO-6-PICOLINE
2-CHLORO-5-NITRO-6-METHYLPYRIDINE
2-CHLORO-5-NITRO-6-PICOLINE
2-CHLORO-6-METHYL-3-NITROPYRIDINE
2-CHLORO-6-METHYL-5-NITROPYRIDINE
6-CHLORO-2-METHYL-3-NITROPYRIDINE
6-CHLORO-3-NITRO-2-METHYLPYRIDINE
6-CHLORO-3-NITRO-2-PICOLINE
6-CHLORO-5-NITRO-2-PICOLINE
TIMTEC-BB SBB003830
TIMTEC-BB SBB003832
2-CHLORO-5-NITRO-6-PICOLINE (2-CHLORO-6-METHYL-5-NITROPYRIDINE)
2-Chloro-5-Nitro-6-methylpyrdine
6-Chloro-2-methyl-3-nitro-pyridine ,97%
[Molecular Formula]

C6H5ClN2O2
[MDL Number]

MFCD03085820
[Molecular Weight]

172.57
[MOL File]

22280-60-0.mol
Chemical PropertiesBack Directory
[Appearance]

Light yellow Cryst
[Melting point ]

54-58 °C
[Boiling point ]

200°C (rough estimate)
[density ]

1.5610 (rough estimate)
[refractive index ]

1.5500 (estimate)
[storage temp. ]

Keep in dark place,Sealed in dry,Room Temperature
[form ]

Powder
[pka]

-3.26±0.10(Predicted)
[color ]

Light beige to brown
[Detection Methods]

HPLC
[InChI]

InChI=1S/C6H5ClN2O2/c1-4-5(9(10)11)2-3-6(7)8-4/h2-3H,1H3
[InChIKey]

GHSRMSJVYMITDX-UHFFFAOYSA-N
[SMILES]

C1(C)=NC(Cl)=CC=C1[N+]([O-])=O
[CAS DataBase Reference]

22280-60-0(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
[Hazard Note ]

Harmful
[HazardClass ]

IRRITANT
[HS Code ]

29333990
Raw materials And Preparation ProductsBack Directory
[Preparation Products]

5-FLUORO-1H-PYRROLO[3,2-B] PYRIDINE-->3-Amino-2-pyridinecarboxylic acid-->3-TERT-BUTOXYCARBONYLAMINO-PYRIDINE-2-CARBOXYLIC ACID-->3-Chloropyridine-2-carboxylic acid-->3-Amino-2-picoline-->3-Bromo-6-chloro-2-methylpyridine-->5-METHOXY-1H-PYRROLO[3,2-B]PYRIDINE-->3-CHLORO-2-METHYLPYRIDINE-->3-NITRO-PYRIDINE-2-CARBOXYLIC ACID-->2-Methyl-3-Nitro-6-Phenoxypyridine-->Pyridine,6-hydrazinyl-2-methyl-3-nitro--->4-(6-METHYL-5-NITRO-2-PYRIDINYL)-1-PIPERAZINECARBOXYLIC ACID 1,1-DIMETHYLETHYL ESTER
Hazard InformationBack Directory
[Chemical Properties]

Light yellow Cryst
[Uses]

6-Chloro-2-methyl-3-nitropyridine has been used as a reactant for the synthesis of fluorine-containing pyridinealdoxime derivatives as treatment of organophosphorus nerve-agent poisoning.
[Preparation]

A mixture of 2-oxo-5-nitro-6-methyl-1,2-dihydropyridine, phosphorous oxychloride, and phosphorous pentachloride was heated at 110° C for 2 hours, whereupon the reaction mixture was charged with an additional portion of phosphorous pentachloride and phosphorous oxychloride. The reaction was stirred for 1 hour and then poured into ice water. The brown solid was filtered and washed with cold water, to give 6-Chloro-2-methyl-3-nitropyridine (94%).
6-Chloro-2-methyl-3-nitropyridine
Spectrum DetailBack Directory
[Spectrum Detail]

6-Chloro-2-methyl-3-nitropyridine(22280-60-0)1HNMR
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

6-Chloro-3-nitro-2-picoline, 98%(22280-60-0)
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