ChemicalBook CAS DataBase List 1-Ethyl-3-methylimidazolium tetrafluoroborate

1-Ethyl-3-methylimidazolium tetrafluoroborate synthesis

8synthesis methods

Product Name:1-Ethyl-3-methylimidazolium tetrafluoroborate
CAS Number:143314-16-3
Molecular formula:C6H11BF4N2
Molecular Weight:197.97

13755-29-8 Synthesis

13755-29-8
469 suppliers
$6.00/25g

65039-09-0 Synthesis

65039-09-0
319 suppliers
$8.00/5g

1-Ethyl-3-methylimidazolium tetrafluoroborate

143314-16-3
264 suppliers
$6.00/5g

Yield:143314-16-3 94%

Reaction Conditions:

at 40; for 18 h;UV-irradiation;Wavelength;

Steps:

1.2; 1.3; 2.2; 2.3

(2) mixing the quaternary ammonium salt solution obtained in the step (1) with sodium tetrafluoroborate (the molar ratio of 1-methylimidazole to sodium tetrafluoroborate is 1:1), After heating to 40 ° C, Under agitation, Irradiation with ultraviolet light of 600 W/m2, The exposure time is 18h, a mixed solution containing a tetrafluoroborate ionic liquid; (3) filtering the mixture obtained in the step (2) twice, Get the filtrate, The filtrate was concentrated at 60 ° C. Remove ethanol, Obtaining 1-ethyl-3-methylimidazolium tetrafluoroborate ionic liquid, The yield was 94%. See Table 1 for the properties of the resulting ionic liquid.

References:

CN109734668,2019,A Location in patent:Page/Page column 9-10

65039-08-9 Synthesis