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ChemicalBook--->CAS DataBase List--->87413-09-0

87413-09-0

87413-09-0 Structure

87413-09-0 Structure
IdentificationMore
[Name]

Dess-Martin periodinane
[CAS]

87413-09-0
[Synonyms]

1,1,1-TRIACETOXY-1,1-DIHYDRO-1,2-BENZIODOXOL-3(1H)-ONE
1,1,1-TRIS(ACETYLOXY)-1,1-DIHYDRO-1,2-BENZIODOXOL-3-(1H)-ONE
1,1-DIHYDRO-1,1,1-TRIACETOXY-1,2-BENZOIODOOXOL-3(1H)-ONE
ACETIC ACID 1,1-DIACETOXY-3-OXO-1L5-IODA-2-OXA-INDAN-1-YL ESTER
DESS-MARTIN
DESS-MARTIN PERIODINANE
DESS-MARTIN REAGENT
DESSS-MARTIN PERIODINANE
RARECHEM AR PA 0035
TRIACETOXYPERIODINANE
Triacetoxyperiodinane (Dess-Martin periodinane)
DESS-MARTIN PERIODINANE, 0.3M SOLUTION &
(7,7-DIACETYLOXY-9-OXO-7$L^{5}-IODA-8-OXABICYCLO[4.3.0]NONA-1,3,5-TRIEN-7-YL) ACETATE
DesmartinPeriodinane
DmpDess-MartinPeriodinane
Dess-Martinperiodinane,97%
Dess-Martin periodinane, 15 wt.% solution in dichloromethane
1,2-Benziodoxol-3(1H)-one, 1,1,1-tris(acetyloxy)-1,1-dihydro-
1,1,1-TRIACETOXY-1,1-DIHYDRO-1,2-BENZIODOXOL-3-(1H)-ONE(DESS-MARTINPERIODINANE)
DESS-MARTINE
[EINECS(EC#)]

672-328-8
[Molecular Formula]

C13H13IO8
[MDL Number]

MFCD00130127
[Molecular Weight]

424.14
[MOL File]

87413-09-0.mol
Chemical PropertiesBack Directory
[Appearance]

White Crystalline powder
[Melting point ]

130-133 °C (lit.)
[Boiling point ]

40 °C
[density ]

1.369 g/mL at 25 °C
[Fp ]

>221 °F
[storage temp. ]

0-6°C
[solubility ]

Soluble in chloroform, acetone, acetonitrile and methylene chloride. Slightly soluble in ether and hexane.
[form ]

Liquid
[color ]

Colorless to light yellow
[Sensitive ]

Light Sensitive
[Merck ]

14,2933
[BRN ]

4548207
[Stability:]

Light Sensitive
[InChI]

InChI=1S/C13H13IO8/c1-8(15)19-14(20-9(2)16,21-10(3)17)12-7-5-4-6-11(12)13(18)22-14/h4-7H,1-3H3
[InChIKey]

NKLCNNUWBJBICK-UHFFFAOYSA-N
[SMILES]

I1(OC(=O)C)(OC(=O)C)(OC(=O)C)OC(=O)C2C=CC=CC1=2
[CAS DataBase Reference]

87413-09-0(CAS DataBase Reference)
[Storage Precautions]

Air sensitive;Store under inert gas;Moisture sensitive
Safety DataBack Directory
[Hazard Codes ]

Xn,O,Xi
[Risk Statements ]

R22:Harmful if swallowed.
R36/37/38:Irritating to eyes, respiratory system and skin .
R40:Limited evidence of a carcinogenic effect.
R8:Contact with combustible material may cause fire.
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
S36/37:Wear suitable protective clothing and gloves .
S24/25:Avoid contact with skin and eyes .
S23:Do not breathe gas/fumes/vapor/spray (appropriate wording to be specified by the manufacturer) .
S17:Keep away from combustible material .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[RIDADR ]

UN 1593 6.1/PG 3
[WGK Germany ]

3
[Hazard Note ]

Harmful/Light sensitive
[TSCA ]

No
[HazardClass ]

5.1
[PackingGroup ]

[HS Code ]

29349900
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Acetic acid-->Acetic anhydride-->p-Toluenesulfonic acid-->Potassium bromate-->2-Iodobenzoic acid-->2-Iodoxybenzoic acid
[Preparation Products]

C-(3,4-DIHYDRO-2H-BENZO[1,4]OXAZIN-3-YL)-METHYLAMINE-->3-Chloro-4-Cyanobenzaldehyde-->3-(4-FLUORO-PHENYL)-1-ISOPROPYL-1H-INDOLE-2-CARBALDEHYDE-->(3-OXO-PROPYL)-CARBAMIC ACID TERT-BUTYL ESTER-->4-FORMYL-N-CBZ-PIPERIDINE-->1-[[(4-METHYLPHENYL)SULPHONYL]OXY]-1,2-BENZIODOXOL-3(1H)-ONE-->1H-Indazole-1-propanoic acid
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

(1,1,1-Triacetoxy)-1,1-dihydro-1,2-benziodoxol-3(1H)-one(87413-09-0).msds
Hazard InformationBack Directory
[Description]

Dess-Martin periodinane (DMP) is a hypervalent iodine compound widely used as a mild reagent for the oxidation of primary/secondary alcohols to aldehydes/ketones; oxidation of amides into imides; the dehydrogenation of amines to nitriles, and disulfides to sulfones. It is also used to selectively oxidize alkenes to epoxides. This is a useful reaction for generating three-membered cyclic ethers. Additionally, DMP is used to oxidatively cleave 1,2-diols to form aldehydes or ketones and in the synthesis of lactones.
[Chemical Properties]

White Crystalline powder
[Uses]

Dess-Martin Periodinaneis a very usefulreagent used in the oxidation of primary alcohols to aldehydes and secondary alcohols to ketones.
[Uses]

Oxidizing reagent.
[reaction suitability]

reagent type: oxidant
[Advantages]

Benefits of using Dess-Martin periodinane (DMP) as an oxidizing reagent:
milder reaction conditions (room temperature, neutral pH)
shorter reaction times and higher yields
high chemoselectivity
tolerance of sensitive functional groups, and a long shelf life
simplified workups
Spectrum DetailBack Directory
[Spectrum Detail]

Dess-Martin periodinane(87413-09-0)IR1
Dess-Martin periodinane(87413-09-0)IR2
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

Dess-Martin periodinane, 15 wt.% solution in dichloromethane(87413-09-0)
[Alfa Aesar]

Dess-Martin periodinane(87413-09-0)
[Sigma Aldrich]

87413-09-0(sigmaaldrich)
[TCI AMERICA]

Dess-Martin Periodinane,>95.0%(T)(87413-09-0)
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