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ChemicalBook--->CAS DataBase List--->15658-60-3

15658-60-3

15658-60-3 Structure

15658-60-3 Structure
IdentificationMore
[Name]

Diethyl 2,6-pyridinedicarboxylate
[CAS]

15658-60-3
[Synonyms]

2,6-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER
DIETHYL 2,6-PYRIDINEDICARBOXYLATE
DIETHYL DIPICOLINATE
DIPICOLINIC ACID DIETHYL ESTER
RARECHEM AL BI 0203
Pyridinedicarboxylicaciddiethylester
diethyl pyridine-2,6-dicarboxylate
PYRIDINE-2,6-DICARBOXYLIC ACID DIETHYL ESTER
2,6-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER 98+%
2,6-Pyridinedicarboxylic acid diethyl ester ,99%
[Molecular Formula]

C11H13NO4
[MDL Number]

MFCD00033792
[Molecular Weight]

223.23
[MOL File]

15658-60-3.mol
Chemical PropertiesBack Directory
[Melting point ]

44°C
[Boiling point ]

188 °C / 12mmHg
[density ]

1.165±0.06 g/cm3(Predicted)
[storage temp. ]

Inert atmosphere,Room Temperature
[pka]

-0.20±0.10(Predicted)
[Detection Methods]

GC,T,NMR
[CAS DataBase Reference]

15658-60-3(CAS DataBase Reference)
Safety DataBack Directory
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[HS Code ]

29333990
Hazard InformationBack Directory
[Chemical Properties]

Yellow to red crystalline powder
[Synthesis]

Pyridine-2,6-dicarboxylic acid (10.0g, 59.9mmol) was added into ethanol (120mL), then 3 drops of concentrated sulfuric acid were added. The mixture was heated to reflux for 8 hours. After evaporation of the solvent, the solid residue was washed with saturated Na2CO3 aqueous solution and extracted with chloroform for 3 times. The organic phase was dried with small amount of MgSO4. The solvent was removed to afford 1 as white powder (12.6g, 56.3mmol, yield = 94%). 1 H-NMR (400MHz, CDCl3) |? ppm 8.29 (d, J = 7.80 Hz, 2H), 8.01 (t, J = 7.80, 7.80 Hz, 1H), 4.50 (q, J = 7.12, 7.12, 7.12 Hz, 2H), 1.47 (t, J = 7.13, 7.13 Hz, 3H). 13C-NMR (100 MHz, CDCl3) |? ppm 164.6, 148.6, 138.2,127.8, 62.3,14.2,14.2. ESI MS: m/z = 224.1 [M+H]+ , 246.1 [M+Na]+ .
Synthesis_15658-60-3
Spectrum DetailBack Directory
[Spectrum Detail]

Diethyl 2,6-pyridinedicarboxylate(15658-60-3)MS
Diethyl 2,6-pyridinedicarboxylate(15658-60-3)1HNMR
Diethyl 2,6-pyridinedicarboxylate(15658-60-3)13CNMR
Diethyl 2,6-pyridinedicarboxylate(15658-60-3)IR1
Diethyl 2,6-pyridinedicarboxylate(15658-60-3)IR2
Well-known Reagent Company Product InformationBack Directory
[TCI AMERICA]

Diethyl 2,6-Pyridinedicarboxylate,>98.0%(GC)(T)(15658-60-3)
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