成人免费xx,国产又黄又湿又刺激不卡网站,成人性视频app菠萝网站,色天天天天

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List Phenylacetyl disulfide
15088-78-5

Phenylacetyl disulfide synthesis

2synthesis methods
-

Yield:15088-78-5 55%

Reaction Conditions:

with iodine in ethanol at 20; for 12 h;

Steps:

Synthesis of diacyl disulfides
General procedure: Diacyl disulfides were synthesized using a modified procedure from the corresponding thioacids.2 Briefly, the thioacid (2 mmol) was dissolved in EtOH (20 ml). To this solution iodine (2 mmol) was added at room temperature. The reaction was stirred under room temperature for 12 hours. EtOH was removed under reduced pressure and ethyl acetate was added into the residue. The mixture was then washed by 10% Na2CO3,brine, dried w/MgSO4, then subjected to flash chromatography to afford the product.

References:

Parent, Zoel;Wang, Yingying;Xian, Ming;Xu, Shi [Bioorganic and Medicinal Chemistry Letters,2020,vol. 30,# 4,art. no. 126903] Location in patent:supporting information

FullText

Phenylacetyl disulfide Related Search: