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ChemicalBook CAS DataBase List METHYLVINYLTHIOETHER
1822-74-8

METHYLVINYLTHIOETHER synthesis

10synthesis methods
-

Yield:-

Reaction Conditions:

with sodium sulfide;sodium hydroxide in water;

Steps:

EXPERIMENTAL

Methyl vinyl sulfide was synthesized in 60% yieldby an original procedure that comprised reductivevinylation of dimethyl sulfoxide with acetylene in thepresence of the Na2S-4H2O-NaOH system [13, 14]and purified by fractionation, bp 64°C (720 mmHg).Characteristics of the monomer corresponded to publisheddata [15]: 1.4843, 0.9026

References:

Markova;Tatarinova;Apartsin;Kireeva;Trofimov [Doklady Chemistry,2019,vol. 489,# 2,p. 288 - 291][Dokl. Akad. Nauk,2019,vol. 489,# 5]