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ChemicalBook CAS DataBase List Ethyl caprylate
106-32-1

Ethyl caprylate synthesis

13synthesis methods
Usually prepared by esterification of caprylic acid with ethyl alcohol and sulfuric acid as catalyst; also by alcoholysis of coconut oil in the presence of HCl.
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Yield:106-32-1 95.1%

Reaction Conditions:

with TiO2-doped zirconia for 6 h;Reflux;

Steps:

1.1; 2.1; 3.1; 4-6; 1; 2 1) Preparation of ethyl n-octanoate:

After mixing 1.3 kg of n-octanoic acid and 0.5 kg of ethanol, add 0.006 kg of solid super acid, heat to reflux for 6 hours, and filter to obtain precipitate and filtrate.Distill the filtrate under reduced pressure to obtain ethyl n-octanoate;

References:

CN112279784,2021,A Location in patent:Paragraph 0034-0045

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