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ChemicalBook CAS DataBase List Cyclohexene oxide
286-20-4

Cyclohexene oxide synthesis

14synthesis methods
-

Yield:286-20-4 98%

Reaction Conditions:

with tert.-butylhydroperoxide;C10H10MoN2O7 in water;1,2-dichloro-ethane at 80;Overall yield = 78percent;Reagent/catalyst;

Steps:

2.4.2 Epoxidation reactions
General procedure: The catalytic abilities of all complexes were studied for epoxidation of alkenes, i.e. styrene and cyclohexene, and monoterpenes, i.e. S(-)-limonene and (-)-α-pinene, using aqueous 30% H2O2 or 5.5M decane solution of tert-butyl hydroperoxide. Different amounts of catalysts and oxidants were also tested to optimize reaction conditions. All reactions were run in 1,2-dichloroethane (DCE) at 80°C and monitored by GC using 1:100:200M ratio of catalyst, substrate and oxidant, respectively. The yields were recorded as GC yield based on the starting substrate. The identity of oxidation products were confirmed by GC-MS.

References:

Karman, Marta;Romanowski, Grzegorz;Wera, Micha? [Polyhedron,2020,vol. 187]

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