ChemicalBook CAS DataBase List Bisphenol A bisallyl ether

Bisphenol A bisallyl ether synthesis

15synthesis methods

Product Name:Bisphenol A bisallyl ether
CAS Number:3739-67-1
Molecular formula:C21H24O2
Molecular Weight:308.41

Bisphenol A bisallyl ether can be obtained from bisphenol A and KOH through a series of operations.

620-92-8 Synthesis

620-92-8
251 suppliers
$8.00/250mg

107-05-1 Synthesis

107-05-1
411 suppliers
$16.80/100ML

3739-67-1
136 suppliers
$73.00/100mg

Yield:3739-67-1 312.8 g

Reaction Conditions:

Stage #1: bis-(4-hydroxyphenyl)methanewith potassium carbonate in N,N-dimethyl-formamide at 100; for 6 h;
Stage #2: 3-chloroprop-1-ene at 85; for 7 h;

Steps:

3

This embodiment provides a process for the azeotropic synthesis of bisphenol F diallyl ether using bisphenol F and 3-chloropropene. The preparation method includes the steps of dissolving 200.2 g of bisphenol F in 400 g of DMF, Add 138.2g of potassium carbonate and react at 100°C for 6h until complete reaction to produce phenate. And after the reaction, vacuum dehydration, add 175.5g of 3-chloropropene to the phenate after dehydration, Raise the temperature to 85°C and keep the reaction temperature for 7 hours. After stopping the reaction, filter the by-products. The unreacted 3-chloropropene and solvent are distilled out to obtain bisphenol F diallyl ether. After measurement, the mass of the product obtained is 281.6g, The purity of bisphenol F diallyl ether in the product was 89.33%.

References:

CN112125787,2020,A Location in patent:Paragraph 0025-0026

80-05-7 Synthesis