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ChemicalBook CAS DataBase List ACIVICIN
42228-92-2

ACIVICIN synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 9 steps
1: Cl2, H2SO4 / 5 h / Irradiation
2: 85 percent / pH 9
3: 85 percent / dicyclohexylcarbodiimide / ethyl acetate / 0 °C
4: tetrahydrofuran / -50 - -30 °C
5: hydroxylamine / H2O / pH 6
6: Et3N / H2O / Ambient temperature; pH 11
7: tetrahydrofuran
8: 54 percent / dichlorotris(dimethylamino)phosphorane / tetrahydrofuran / Heating
9: 87 percent / trifluoroacetic acid, thioanisole

References:

Silverman, Richard B.;Holladay, Mark W. [Journal of the American Chemical Society,1981,vol. 103,# 24,p. 7357 - 7358]

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