ChemicalBook CAS DataBase List 9-Bromo-10-(2-naphthyl)anthracene

9-Bromo-10-(2-naphthyl)anthracene synthesis

11synthesis methods

Product Name:9-Bromo-10-(2-naphthyl)anthracene
CAS Number:474688-73-8
Molecular formula:C24H15Br
Molecular Weight:383.28

128-08-5 Synthesis

128-08-5
843 suppliers
$5.00/5G

7424-72-8
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$75.00/100mg

474688-73-8
224 suppliers
$15.00/1g

Yield:474688-73-8 99%

Reaction Conditions:

in water;N,N-dimethyl-formamide;

Steps:

S.5 Synthesis Example 5

Synthesis Example 5 (Synthesis of 9-bromo-10-(naphthalene-2-yl)anthracene) 23.1 g of 9-(naphthalene-2-yl)anthracene was dispersed into 250 ml of DMF (dimethylformamide), and then 14.9 g of NBS (N-bromosuccinimide) in DMF solution (150 ml) was dropped therein. After stirred at room temperature for 7 hours, it was left over a night. 200 ml of water was added thereto, and then the crystal precipitated was separated by filtration. Subsequently it was washed by ethanol adequately, followed by drying, and 28.8 g of 9-bromo-10-(naphthalene-2-yl)anthracene of beige color crystal was obtained (Yield: 99%).

References:

US2007/152565,2007,A1

523-27-3 Synthesis