(5-acetyloxy-3,4-dibenzoyloxy-oxolan-2-yl)methyl benzoate synthesis
- Product Name:(5-acetyloxy-3,4-dibenzoyloxy-oxolan-2-yl)methyl benzoate
- CAS Number:70832-64-3
- Molecular formula:C28H24O9
- Molecular Weight:504.48
6974-32-9
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70832-64-3
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67525-66-0
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7408-41-5
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79439-67-1
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Yield:70832-64-3 9.5% ，7408-41-5 40% ，67525-66-0 8% ，79439-67-1 8%
Reaction Conditions:
with trimethylsilylazide in dichloromethane at 20; for 3 h;Further byproducts given;Rearrangement;azidation; deacetylation;
References:
Stimac, Anton;Kobe, Joze [Carbohydrate Research,2000,vol. 324,# 3,p. 149 - 160]