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ChemicalBook CAS DataBase List 4-(trans-4-Pentylcyclohexyl)benzoic acid
65355-30-8

4-(trans-4-Pentylcyclohexyl)benzoic acid synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 2.) 10percent aq. HCl / 1.) diethyl ether, 1 h, heating
2: p-toluenesulfonic acid / toluene / Heating
3: H2 / 10percent Pd/C / ethanol
4: AlCl3 / 1,2-dichloro-ethane / 0.5 h
5: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C

References:

Bezborodov, V. S.;Bubel', O. N.;Konovalov, V. A.;Ptashnikov, Yu. L. [Journal of Organic Chemistry USSR (English Translation),1983,vol. 19,p. 1479 - 1483][Zhurnal Organicheskoi Khimii,1983,vol. 19,# 8,p. 1669 - 1674]

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