3-FLUORO-4-NITROBENZYL BROMIDE synthesis
- Product Name:3-FLUORO-4-NITROBENZYL BROMIDE
- CAS Number:131858-37-2
- Molecular formula:C7H5BrFNO2
- Molecular Weight:234.02
503315-74-0
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Yield: 75%
Reaction Conditions:
with N-Bromosuccinimide;triphenylphosphine in dichloromethane at 20; for 2 h;Product distribution / selectivity;
Steps:
6.A
Part A. Preparation of 4-(bromomethyl)-2-fluoro- 1 -nitrobenzene.; [00539] (3-Fluoro-4-nitrophenol)methanol (1.24g, 7.25mmol) was dissolved in dichloromethane (25mL) and treated with triphenylphosphine (2.281g, 8.70mmol) followed by N-bromosuccinimide (1.548g,
References:
Location in patent:Page/Page column 110-111
446-34-4
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131858-37-2
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$65.00/500mg