2-萘胺(91-59-8)紅外圖譜(IR2)
InChI:InChI=1S/C10H9N/c11-10-6-5-8-3-1-2-4-9(8)7-10/h1-7H,11H2
InChIKey: JBIJLHTVPXGSAM-UHFFFAOYSA-N
Smiles:C1=C2C(C=CC=C2)=CC=C1N
-
Mass
MS-NW-8694
2-naphthylamine
C10H9N (Mass of molecular ion: 143)
Source Temperature: 270 °C
Sample Temperature: 150 °C
Reservoir, 75 eV
39.0 1.7
50.0 1.1
51.0 1.5
57.5 1.7
58.5 3.5
62.0 1.4
63.0 3.2
65.0 1.8
70.5 4.1
71.5 7.2
74.0 1.0
75.0 1.2
76.0 1.0
77.0 1.0
88.0 1.1
89.0 3.8
113.0 1.5
114.0 2.5
115.0 33.2
116.0 17.7
117.0 2.7
126.0 2.1
140.0 1.5
141.0 1.1
142.0 4.2
143.0 100.0
144.0 11.6
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C10 H9 N
|
0.044 g : 0.5 ml CDCl3
|
| 2-naphthylamine
|
 |
Assign. Shift(ppm)
A *1 7.674
B 7.627
C *1 7.566
D *2 7.350
E *2 7.210
F 6.925
G 6.892
J 3.76
J(F,G)=2.3HZ. J(B,G)=8.5HZ.
|
Hz ppm Int.
3077.88 7.702 37
3071.29 7.685 569
3070.68 7.684 582
3067.38 7.676 72
3063.11 7.665 619
3062.50 7.663 631
3057.62 7.651 58
3052.86 7.639 799
3049.32 7.630 60
3044.07 7.617 830
3035.89 7.597 30
3035.52 7.596 31
3028.32 7.578 552
3027.71 7.576 554
3020.02 7.557 656
3019.41 7.556 655
2948.73 7.379 40
2945.43 7.371 415
2944.21 7.367 434
2941.65 7.361 64
2938.60 7.353 533
2937.26 7.350 783
2935.91 7.347 385
2930.42 7.333 436
2929.08 7.330 426
2892.70 7.239 45
2889.40 7.230 548
2888.18 7.227 562
2882.57 7.213 473
2881.23 7.210 884
2880.00 7.207 547
2877.08 7.200 50
2874.39 7.193 425
2781.13 6.959 40
2780.27 6.957 39
2778.81 6.954 45
2775.63 6.946 39
2768.92 6.929 757
2766.72 6.923 1000
2762.21 6.912 76
2759.40 6.905 987
2757.08 6.899 648
2750.85 6.884 866
2748.54 6.878 671
1501.10 3.757 187
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| 1H NMR |
89.56 MHz |
| C10 H9 N
|
0.042 g : 0.5 ml CDCl3
|
| 2-naphthylamine
|
|
Assign. Shift(ppm)
A 7.65
B 7.61
C 7.57
D *1 7.33
E *1 7.21
F 6.91
G 6.86
J 3.68
|
Hz ppm Int.
691.13 7.717 141
690.50 7.710 150
689.38 7.698 124
689.00 7.694 114
688.31 7.686 110
687.00 7.671 192
686.44 7.665 236
685.75 7.657 163
684.56 7.644 161
683.94 7.637 279
683.19 7.629 236
682.63 7.623 213
681.81 7.613 313
681.00 7.604 262
680.44 7.598 194
679.63 7.589 200
676.56 7.555 282
674.94 7.537 154
673.88 7.525 200
672.81 7.513 269
672.19 7.506 250
665.13 7.427 154
663.44 7.408 189
658.44 7.352 363
656.81 7.334 260
655.31 7.317 62
651.19 7.271 464
649.13 7.248 437
644.56 7.197 141
643.44 7.185 231
642.44 7.174 118
641.75 7.166 234
636.81 7.111 113
635.13 7.092 94
620.69 6.931 38
618.63 6.908 1000
617.06 6.890 266
616.69 6.886 253
616.25 6.881 248
611.13 6.824 340
608.81 6.798 192
329.75 3.682 199