N-Phenyl-bis(trifluoromethanesulfonimide)

37595-74-7

CAS-Nr.: 37595-74-7

Englisch Name:: N-Phenyl-bis(trifluoromethanesulfonimide)

Synonyma:: PHENYL TRIFLIMIDE;N,N-BIS(TRIFLUOROMETHYLSULFONYL)ANILINE;N-PHENYLBIS(TRIFLUOROMETHANESULFONIMIDE);1,1,1-trifluoro-N-phenyl-N-trifluoromethanesulfonylmethanesulfonamide;N-PHENYLTRIFLUOROMETHANESULFONIMIDE;phenyltrifluoromethanesulfonimide;N-PHENYLBIS(TRIFLUOROMETHANESULPHONIMIDE);trifluoro-N-phenyl-N-(trifluoromethylsulfonyl)methanesulfonamide;N-PHENYLT;NSC 240874

CBNumber:: CB5289550

Summenformel:: C8H5F6NO4S2

Molgewicht:: 357.25

MOL-Datei:: 37595-74-7.mol

Request For Quotation

Eigenschaften Sicherheit Verwendungswort Produktionsfirma 512

N-Phenyl-bis(trifluoromethanesulfonimide) Eigenschaften

Schmelzpunkt:: 100-102 °C(lit.)

Siedepunkt:: 305.3±52.0 °C(Predicted)

Dichte: 1.766±0.06 g/cm3(Predicted)

storage temp.: Keep in dark place,Sealed in dry,Room Temperature

L?slichkeit: Soluble in methanol. Slightly soluble in chloroform and ethyl acetate.

pka: -13.12±0.50(Predicted)

Aggregatzustand: Crystals or Crystalline Powder

Farbe: White or colorless

Sensitive: Moisture Sensitive

BRN: 1269141

Stabilit?t:: Moisture Sensitive

InChI: InChI=1S/C8H5F6NO4S2/c9-7(10,11)20(16,17)15(6-4-2-1-3-5-6)21(18,19)8(12,13)14/h1-5H

InChIKey: DIOHEXPTUTVCNX-UHFFFAOYSA-N

SMILES: C(F)(F)(F)S(N(C1=CC=CC=C1)S(C(F)(F)F)(=O)=O)(=O)=O

CAS Datenbank: 37595-74-7(CAS DataBase Reference)

NIST chemische Informationen: N-phenyltrifluoromethanesulfonimide(37595-74-7)

Sicherheit

Risiko- und Sicherheitserkl?rung
Gefahreninformationscode (GHS)

Kennzeichnung gef?hrlicher	Xi
R-S?tze:	36/37/38
S-S?tze:	26-36
WGK Germany	3
F	21
TSCA	No
HazardClass	IRRITANT
HS Code	29242100

Bildanzeige (GHS)

Alarmwort

Warnung

Gefahrenhinweise

Code	Gefahrenhinweise	Gefahrenklasse	Abteilung	Alarmwort	Symbol	P-Code
H315	Verursacht Hautreizungen.	Hautreizung	Kategorie 2	Warnung	src="/GHS07.jpg" width="20" height="20" />	P264, P280, P302+P352, P321,P332+P313, P362
H319	Verursacht schwere Augenreizung.	Schwere Augenreizung	Kategorie 2	Warnung	src="/GHS07.jpg" width="20" height="20" />	P264, P280, P305+P351+P338,P337+P313P
H335	Kann die Atemwege reizen.	Spezifische Zielorgan-Toxizit?t (einmalige Exposition)	Kategorie 3 (Atemwegsreizung)	Warnung	src="/GHS07.jpg" width="20" height="20" />

Sicherheit

P261	Einatmen von Staub vermeiden.
P264	Nach Gebrauch gründlich waschen.
P264	Nach Gebrauch gründlich waschen.
P271	Nur im Freien oder in gut belüfteten R?umen verwenden.
P280	Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.
P302+P352	BEI BERüHRUNG MIT DER HAUT: Mit viel Wasser/... (Hersteller kann, falls zweckm??ig, ein Reinigungsmittel angeben oder, wenn Wasser eindeutig ungeeignet ist, ein alternatives Mittel empfehlen) waschen.
P305+P351+P338	BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach M?glichkeit entfernen. Weiter spülen.

N-Phenyl-bis(trifluoromethanesulfonimide) Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.

S-S?tze Betriebsanweisung:

S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.
S36:DE: Bei der Arbeit geeignete Schutzkleidung tragen.

Beschreibung

N-Phenylbis(trifluoromethanesulfonimide) acts as a mild triflating reagent as well as a transparent strong electron-withdrawing p-type dopant in carbon nanotubes. It is also employed as a reactant for the preparation of amphoteric alfa-boryl aldehydes. It plays an important role in the enantioselective synthesis of the core ring skeleton of leucosceptroids A-D and in steroselective sulfoxidation.

Chemische Eigenschaften

white to off-white crystalline powder

Synthese

Add methylene chloride, aniline, 4-dimethylaminopyridine (DMAP), and triethylamine to a reactor equipped with a thermometer, distillation device, and mechanical stirring. When the vacuum of the reactor is evacuated to -0.095MPa and cooled to -40°C, trifluoromethanesulfonyl fluoride gas is introduced and then stirred at -20°C ~ 0°C and 0.02MPa ~ 0.1MPa reaction pressure, and react for 6 hours Finally, the excess trifluoromethanesulfonyl fluoride gas in the reactor is released and collected by cooling. After the inside of the reactor is brought to normal pressure, 500 mL of water is added, and the liquid is separated. A light yellow solid is obtained after the organic phase is heated to 40°C and methylene chloride is distilled. The light yellow solid is recrystallized with toluene to obtain 650g of white crystal N-Phenyl-bis(trifluoromethanesulfonimide).

N-Phenyl-bis(trifluoromethanesulfonimide) Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Natriumhydrid Ethanol Natriumchlorid Trifluormethansulfonylchlorid Kaliumcarbonat Trifluormethansulfonsaeureanhydrid N,N-Diethylethanamin Tetrahydrofuran Anilin Dichlormethan Natriumhydroxid Magnesiumsulfat

Downstream Produkte

1-Boc-4-methanesulfonyloxypiperidine 2-(triMethylsilyl)ethyl 4-(trifluoroMethylsulfonyloxy)-5,6-dihydropyridine-1(2H)-carboxylate 1-CYCLOHEXEN-1-YL TRIFLUOROMETHANE- Methyl 3-((Trifluoromethylsulfonyl)oxy)phenylacetate

N-Phenyl-bis(trifluoromethanesulfonimide) Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 512)Lieferanten

Firmenname	Telefon	E-Mail	Land	Produktkatalog	Edge Rate
JIANGXI TIME PHARMACEUTICAL CO.,LTD	+86-0794-7183888 +86-13155888520	sales@groupchem.com	China	27	58
Fluoropharm Co., Ltd.	+86-0571-85586753; +8613336034509	sales@fluoropharm.com	China	1376	60
SHANGHAI T&W PHARMACEUTICAL CO., LTD.	+86-021-61551413 +8618813727289	contact@trustwe.com	China	5738	58
Hebei Weibang Biotechnology Co., Ltd	+8615531157085	abby@weibangbio.com	China	8810	58
Hebei Mojin Biotechnology Co., Ltd	+86 13288715578 +8613288715578	sales@hbmojin.com	China	12835	58
Hebei Weibang Biotechnology Co., Ltd	+8617732866630	bess@weibangbio.com	China	18151	58
Zibo Hangyu Biotechnology Development Co., Ltd	+86-0533-2185556 +8617865335152	Mandy@hangyubiotech.com	China	10986	58
Hebei Zhuanglai Chemical Trading Co Ltd	+86-16264648883 +86-16264648883	niki@zlchemi.com	China	2691	58
Capot Chemical Co.,Ltd.	+86-（0）57185586718 +86-13336195806	sales@capot.com	China	29791	60
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	18751	58

37595-74-7()Verwandte Suche:

Chlortriphenylmethan Phthalimid Lithiumbis(trifluormethyl-sulfonyl)imid Anilin Succinimid 1,1'-(Methylendi-p-phenylen)bismaleimid Trifluormethansulfonylchlorid TRIFLUOROMETHANESULFONIMIDE Dimethylsulfon N-Phenylethylendiamin 1-Iodpyrrolidin-2,5-dion 1-Phenyl-1H-pyrrol-2,5-dion N-Phenylmethacrylamid N-Phenylanthranilsure N-Phenyl-1-naphthalinamin N-Phenylcarbazol Kalium-N-phenylglycinat 1-Phenylpiperidin

1,1,1-TRIFLUORO-N-PHENYL-N-[(TRIFLUOROMETHYL)SULFONYL]METHANESULFONAMIDE
N-Phenylbis(trifluoromethanesulphonimide), Phenyl triflimide
N-Phenyl bis trifluorosulphonamide
N-Bis(trifluoromethylsulfonyl)aniline
1,1,1-trifluoro-N-(methylsulfonyl)methanesulfonamide
N- phenyl-bis (trifluoromethanesulfonyl) imide
N-Phenylbis(trifluoroMethanesulfoniMide), 97% 5GR
N,N-Bis(trifluoromethylsulfonyl)aniline Phenyl Triflimide N-Phenyltrifluoromethanesulfonimide
N,N-Bis(trifluoroMethylsufonyl)aniline
N,N-Bis(trifluoroMethylsulfonyl)aniline SynonyMs N-Phenylbis(trifluoroMethanesulfon)iMide
N-phenyldouble(threefluoro Methanesulfonic acidiMide
N-Phenyl-bis(trifluoroMethanesulfoniMide) >=98.0% (HPLC)
N,N-Bis(trifluoromethanesulphonyl)aniline~Phenyl triflimide~N-Phenyltrifluoromethanesulphonimide
Phenyl triflimide~N-Phenyltrifluoromethanesulphonimide
N-PHENYL-BIS-(TRIFLUORMETHANSULFONIMID)
N,N-BIS-(TRIFLUOROMETHANESULFONYL)ANILINE
1,1,1-Trifluoro-N-phenyl-N-(trifluoromethyl)sulphonylmethanesulphonamide
n-phenylbis(trifluorometanesulfonimide)
N-Phenyl-bis(trifluoromethyl)sulfonimide
N-Phenylbis(trifluoromethanesulfonimide) [Triflating Reagent]
N-phenyl-bis(trifluoromethanesulfonamide)
N,N-Bis(trifluoromethylsulfonyl)aniline, N-Phenyl-trifluoromethanesulfonimide, Phenyl triflimide, 1,1,1-Trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]methanesulfonamide
N-Phenyltrifluoromethanesulfonimide ,98%
N-Phenyl-bis(trifluoromethanesulfonimide),1,1,1-Trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]methanesulfonamide, N,N-Bis(trifluoromethylsulfonyl)aniline, N-Phenyl-trifluoromethanesulfonimide, Pheny
N,N-Bis(trifluoromethylsulphonyl)aniline 98%
N-Phenylbis(trifluoromethanesulfonyl)amine
N-Phenylbis(trifluoromethylsulfonyl)amine
N-Phenyl-N,N-bis(trifluoromethylsulfonyl)amine
N-Phenylbis(trifluoromethanesulphonimide)97%
N-Phenylbis(trifluoromethanesulfonimide),97%
N-Phenylbis(trifluromethanesulphonimide)99%
N-phenyl bis(trifluoromethanesulfonyl)amide
N-Phenyl-bis(trifluoromethanesulfonimide) 37595-74-7
N,N-Bis(trifluoromethylsulfonyl)aniline 37595-74-7
-bis(trifL
fonimide)
N-Phenylbis(trifluoromethanesulfonimide)[TriflatingReagent]>
Methanesulfonamide, 1,1,1-trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]-
1,1,1-trifluoro-N-phenyl-N
TIANFUCHEM--37595-74-7--N-Phenyl-bis(trifluoromethanesulfonimide) factory price
phenyltrifluoromethanesulfonimide
N-PHENYLBIS(TRIFLUOROMETHANESULFONIMIDE)
N-PHENYLBIS(TRIFLUOROMETHANESULPHONIMIDE)
N-PHENYLTRIFLUOROMETHANESULFONIMIDE
N-PHENYLTRIFLUOROMETHANESULPHONIMIDE
N,N-BIS(TRIFLUOROMETHYLSULFONYL)ANILINE
NSC 240874
1,1,1-trifluoro-N-phenyl-N-trifluoromethanesulfonylmethanesulfonamide
PHENYL TRIFLIMIDE
trifluoro-N-phenyl-N-(trifluoromethylsulfonyl)methanesulfonamide
N-PHENYLT
Bis(trifluoromethylsulfonyl)aniline
N- phenylbis (trifluoromethanesulfonyl) imine
N-PHENYL-BIS(TRIFLUROMETHANSULPHONIMIDE)
N-phenylbis (trifluoromesulfonimide)
N,N-Bis(trifluoromethylsulfonyl)aniline, N-Phenyl-trifluoromethanesulfonimide
37595-74-7
7595-74-7

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