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ChemicalBook--->CAS DataBase List--->39262-22-1

39262-22-1

39262-22-1 Structure

39262-22-1 Structure
IdentificationMore
[Name]

L(-)-10-Camphorsulfonyl chloride
[CAS]

39262-22-1
[Synonyms]

(-)-10-CAMPHORSULFONYL CHLORIDE
(1R)-(-)-10-CAMPHORSULFONYL CHLORIDE
(1R)-(-)-CAMPHOR-10-SULFONIC ACID CHLORIDE
(1R)-CAMPHOR-10-SULFONIC ACID CHLORIDE
(1R)-(-)-CAMPHOR-10-SULFONYL CHLORIDE
(1R)-(-)-CAMPHOR-10-SULPHONYL CHLORIDE
(-)-CAMPHOR-10-SULFONYL CHLORIDE
L(-)-10-CAMPHORSULFONYL CHLORIDE
(1R)-(-)-10-CAMPHORSULFONYL CHLORIDE, 97 %
(1R)-(-)-CAMPHOR-10-SULFONIC ACID CHLORIDE 98+%
6,(1R)-(-)-10-Camphorsulfonylchloride
Bicyclo2.2.1heptane-1-methanesulfonyl chloride, 7,7-dimethyl-2-oxo-, (1R,4S)-
(-)-Camphor-10-sulphonyl chloride
(-)-Camphor-10-sulfonyl chloride, (1R)-Camphor-10-sulfonic acid chloride
(7,7-Dimethyl-2-oxo-1-bicyclo[2.2.1]heptanyl)methanesulfonyl chloride
(1R,4S)-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfochloride
[1R,4R,(-)]-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfonic acid chloride
[EINECS(EC#)]

628-057-2
[Molecular Formula]

C10H15ClO3S
[MDL Number]

MFCD00064155
[Molecular Weight]

250.74
[MOL File]

39262-22-1.mol
Chemical PropertiesBack Directory
[Appearance]

white to light yellow crystal powde
[Melting point ]

66-68 °C(lit.)
[alpha ]

-33 º (c=3, chloroform)
[Boiling point ]

349.4±15.0 °C(Predicted)
[density ]

1.331±0.06 g/cm3(Predicted)
[storage temp. ]

2-8°C
[solubility ]

Acetone, Dichloromethane, Ethyl Acetate, Methanol
[form ]

Solid
[color ]

White
[optical activity]

[α]18/D 33°, c = 3 in chloroform
[Water Solubility ]

Decomposes
[Sensitive ]

Moisture Sensitive
[Usage]

A useful synthetic intermediate. Used for asymmetric hydroxylation
[BRN ]

3205975
[InChIKey]

BGABKEVTHIJBIW-UHFFFAOYSA-N
[CAS DataBase Reference]

39262-22-1(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

C
[Risk Statements ]

R34:Causes burns.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
[RIDADR ]

UN 3261 8/PG 2
[WGK Germany ]

3
[F ]

10-21
[HazardClass ]

8
[PackingGroup ]

II
[HS Code ]

29147090
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

(1R)-Camphor-10-sulfonic acid chloride(39262-22-1).msds
Hazard InformationBack Directory
[Chemical Properties]

white to light yellow crystal powde
[Uses]

A chiral derivative of Camphor
[Uses]

L(-)-10-Camphorsulfonyl chloride is a useful synthetic intermediate,it is used for asymmetric hydroxylation.
[Purification Methods]

If free from OH bands in the IR, then recrystallise it from Et2O or pet ether; otherwise treat it with SOCl2 at 50o for 30minutes, evaporate, dry the residue over KOH in a vacuum and recrystallise it. The (±)-acid chloride has m 85o [Bartlett & Knox Org Synth 45 14 1965]. Itis characterised as the amide (prisms from EtOH) m 132o, [ ] 17 (+) and (-) 1.5o (EtOH). On repeated recrystallisation from EtOH the anilide has m 120.5-121o, [] 25 +76o (c 1, CHCl3). [Read & Storey J Chem Soc 2761 1930, Sutherland & Shriner J Am Chem Soc 58 62 1936, Halterman et al. J Am Chem Soc 109 8105 1987, Bartlet & Knox Org Synth 45 55 1945, Beilstein 11 IV 650.]
Spectrum DetailBack Directory
[Spectrum Detail]

L(-)-10-Camphorsulfonyl chloride(39262-22-1)MS
L(-)-10-Camphorsulfonyl chloride(39262-22-1)1HNMR
L(-)-10-Camphorsulfonyl chloride(39262-22-1)IR1
L(-)-10-Camphorsulfonyl chloride(39262-22-1)IR2
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

L(-)-10-Camphorsulfonyl chloride, 97%(39262-22-1)
[Alfa Aesar]

(1R)-(-)-Camphor-10-sulfonyl chloride, 97%(39262-22-1)
[Sigma Aldrich]

39262-22-1(sigmaaldrich)
[TCI AMERICA]

(-)-10-Camphorsulfonyl Chloride,>98.0%(T)(39262-22-1)
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