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ChemicalBook--->CAS DataBase List--->36016-38-3

36016-38-3

36016-38-3 Structure

36016-38-3 Structure
IdentificationMore
[Name]

tert-Butyl N-hydroxycarbamate
[CAS]

36016-38-3
[Synonyms]

BOC-HNOH
BOC-NH-OH
LABOTEST-BB LT00233206
N-BOC-HYDROXYLAMINE
N-HYDROXYCARBAMIC ACID TERT-BUTYL ESTER
N-T-BOC HYDROXYLAMINE
N-(T-BUTOXYCARBONYL)-HYDROXYLAMINE
N-TERT-BUTOXYCARBONYLHYDROXYLAMINE
N-(TERT-BUTYLOXYCARBONYL)HYDROXYLAMINE
T-BUTYL N-HYDROXYCARBAMATE
TERT-BUTYL N-HYDROXYCARBAMATE
N-Boc-hydroxylamine, >=98%
N-tert-Butoxycarbonylhydroxylamine, 98+%
N-(tert-Butoxycarbonyl)hydroxylamine~tert-ButylN-hydroxycarbamate
TERT-BUTYL N-HYDROXYCARBAMATE 99.0%
N-Boc-Hydroxyamine
T-BUTYL N-HYDROXYCARBOMATE (N-BOC HYDROXYLAMINE)
T-BUTYL N-HYDROXYCARBOMATE
PNB(4R,5S,6S)-3-(diphenyloxy)phosphoryloxy-6[(1R)-1-hydoxyethyl]-4-methyl-7-oxo-1-azabicyclo[3,2,0]hept-2-ene-2-caboxylate(MAP or MVP)
(t-Butoxycarbonyl)-hydroxylamine
[EINECS(EC#)]

252-836-2
[Molecular Formula]

C5H11NO3
[MDL Number]

MFCD00002107
[Molecular Weight]

133.15
[MOL File]

36016-38-3.mol
Chemical PropertiesBack Directory
[Appearance]

White to light pink crystalline powder
[Melting point ]

53-55 °C (lit.)
[Boiling point ]

245.66°C (rough estimate)
[density ]

1.2510 (rough estimate)
[refractive index ]

1.4120 (estimate)
[storage temp. ]

2-8°C
[solubility ]

Chloroform, Methanol
[form ]

Crystalline Powder
[pka]

9.31±0.23(Predicted)
[color ]

White to light pink
[Water Solubility ]

Slightly soluble in water.
[Sensitive ]

Moisture Sensitive
[BRN ]

1756546
[InChI]

InChI=1S/C5H11NO3/c1-5(2,3)9-4(7)6-8/h8H,1-3H3,(H,6,7)
[InChIKey]

DRDVJQOGFWAVLH-UHFFFAOYSA-N
[SMILES]

C(OC(C)(C)C)(=O)NO
[CAS DataBase Reference]

36016-38-3(CAS DataBase Reference)
Safety DataBack Directory
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
[WGK Germany ]

3
[F ]

21
[HS Code ]

29280090
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

N-Boc-hydroxylamine(36016-38-3).msds
Hazard InformationBack Directory
[Chemical Properties]

White to light pink crystalline powder
[Uses]

tert-Butyl N-hydroxycarbamate is used in the preparation of azridines by cycloaddition of azides with nitroso Diels-Alder adducts.
[Synthesis Reference(s)]

Journal of the American Chemical Society, 81, p. 955, 1959 DOI: 10.1021/ja01513a049
Tetrahedron Letters, 24, p. 231, 1983 DOI: 10.1016/S0040-4039(00)81372-6
[Synthesis]

A suspension of NH2OH·HCl (9.7 g, 140mmol) and K2CO3 (9.7 g, 700 mmol) in Et2O (60 mL) and H2O (2 mL)was stirred for about 1 h at r.t. with evolution of CO2 gas. A solution of Boc2O (20.0 g, 92 mmol) in Et2O (40 mL) was then added dropwise at 0 °C, and the suspension was stirred at r.t for 12 h. The organic phase was decanted, and the solid was washed with Et2O (3 × 30 mL). The combined organic layers were concentrated, and the residue was recrystallized from cyclohexane/toluene to afford the desired product tert-butyl N-hydroxycarbamate as a white solid.
Spectrum DetailBack Directory
[Spectrum Detail]

tert-Butyl N-hydroxycarbamate(36016-38-3)MS
tert-Butyl N-hydroxycarbamate(36016-38-3)1HNMR
tert-Butyl N-hydroxycarbamate(36016-38-3)13CNMR
tert-Butyl N-hydroxycarbamate(36016-38-3)IR1
tert-Butyl N-hydroxycarbamate(36016-38-3)IR2
tert-Butyl N-hydroxycarbamate(36016-38-3)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

tert-Butyl N-hydroxycarbamate, 98+%(36016-38-3)
[Alfa Aesar]

N-Boc-hydroxylamine, 98+%(36016-38-3)
[Sigma Aldrich]

36016-38-3(sigmaaldrich)
[TCI AMERICA]

tert-Butyl N-Hydroxycarbamate,>98.0%(GC)(36016-38-3)
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