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ChemicalBook--->CAS DataBase List--->33301-41-6

33301-41-6

33301-41-6 Structure

33301-41-6 Structure
IdentificationMore
[Name]

1-(Diphenylmethyl)-3-azetidinyl methanesulfonate
[CAS]

33301-41-6
[Synonyms]

1-BENZHYDRYL-3-METHANESULFONATOAZETIDINE
1-BENZHYDRYL-3-METHANESULFONYLOXY AZETIDINE
1-BENZHYDRYLAZETIDIN-3-YL METHANESULFONATE
1-DIPHENYLMETHYL-3-AZETIDINYL METHANESULFONATE
1-(DIPHENYLMETHYL)-3-(METHANESULFONYLOXY)AZETIDINE
BUTTPARK 37\04-14
1-(diphenylmethyl)-3-(methanesulfonyloxy)azetinide
1-Diphenylmethyl-3-azetidinyl Methanethiosulfonate
1-Benzhydryl-3-methanesulphonyloxyazetidine
1-BENZHYDRYL-3-METHANESULFONATOAZETIDINE 98%
Methanesulfonic acid 1-benzhydryl-azetidin-3-yl ester
1-(Diphenylmethyl)-3-(mesyloxy)azetidine
1-(Diphenylmethyl)-3-[(methylsulfonyl)oxy]azetidine
[EINECS(EC#)]

608-857-8
[Molecular Formula]

C17H19NO3S
[MDL Number]

MFCD00159216
[Molecular Weight]

317.4
[MOL File]

33301-41-6.mol
Chemical PropertiesBack Directory
[Appearance]

White Crystalline Solid
[Melting point ]

111-112°C
[Boiling point ]

459.9±34.0 °C(Predicted)
[density ]

1.28±0.1 g/cm3(Predicted)
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

Dichloromethane, Ether, Ethyl Acetate, Methanol
[form ]

Solid
[pka]

5.67±0.10(Predicted)
[color ]

White
[Usage]

A proline analog and proline formation inhibitor
[InChI]

InChI=1S/C17H19NO3S/c1-22(19,20)21-16-12-18(13-16)17(14-8-4-2-5-9-14)15-10-6-3-7-11-15/h2-11,16-17H,12-13H2,1H3
[InChIKey]

MSVZMUILYMLJCF-UHFFFAOYSA-N
[SMILES]

N1(C(C2=CC=CC=C2)C2=CC=CC=C2)CC(OS(C)(=O)=O)C1
[CAS DataBase Reference]

33301-41-6(CAS DataBase Reference)
Safety DataBack Directory
[Safety Statements ]

24/25
[HazardClass ]

IRRITANT
[HS Code ]

29339900
Hazard InformationBack Directory
[Chemical Properties]

White Crystalline Solid
[Uses]

A proline analog and proline formation inhibitor
[Synthesis]

Preparation procedure of 1-(Diphenylmethyl)-3-azetidinyl methanesulfonate: To a reaction flask was charged 632 g (2.64 mol) of 1-benzhydrylazetidin- 3-ol, acetonitrile (1.9 L), and triethylamine (601 g, 1.5 equiv). The mixture was cooled in an ice-acetone bath (-5 °C). Methanesulfonyl chloride (436 g, 1.20 equiv) was added via a drop funnel while keeping the reaction temperature at less than5 °C. HPLC showed reaction completion after 15 min. Water (6.3 L) was added, and the reaction mixture was stirred for 2 h at room temperature and filtered. The filter cake was rinsed with water (2 x 1 L), pulled dry under vacuum, and directly subjected to the amination reaction in the next step. Yield 100%.
1-(Diphenylmethyl)-3-azetidinyl methanesulfonate synthesis
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

33301-41-6(sigmaaldrich)
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