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ChemicalBook--->CAS DataBase List--->10497-05-9

10497-05-9

10497-05-9 Structure

10497-05-9 Structure
IdentificationMore
[Name]

TRIS(TRIMETHYLSILYL) PHOSPHATE
[CAS]

10497-05-9
[Synonyms]

PHOSPHORIC ACID TRIS(TRIMETHYLSILYL) ESTER
TIMTEC-BB SBB001292
TRIS(TRIMETHYLSILYL) PHOSPHATE
ester
Phosphoric acid, TMS
Phosphoric acid, tristrimethylsilyl
Phosphoric acid, triTMS
Silanol, trimethyl-, phosphate (3:1)
Silanol,trimethyl-,phosphate(3:1)
trimethyl-silanophosphate(3:1)
Tris-(trimethylsilyl)fosfat
Phosphoricacidtrimethylsilylester
[EINECS(EC#)]

234-028-1
[Molecular Formula]

C9H27O4PSi3
[MDL Number]

MFCD00008267
[Molecular Weight]

314.54
[MOL File]

10497-05-9.mol
Chemical PropertiesBack Directory
[Melting point ]

3-4 °C (lit.)
[Boiling point ]

228-229 °C/720 mmHg (lit.)
[density ]

0.945 g/mL at 25 °C(lit.)
[vapor pressure ]

23.3hPa at 20℃
[refractive index ]

n20/D 1.409(lit.)
[Fp ]

76 °F
[storage temp. ]

Inert atmosphere,2-8°C
[form ]

liquid
[pka]

23-25(at 25℃)
[color ]

Colorless to Light yellow to Light orange
[Specific Gravity]

0.959
[Water Solubility ]

935.5μg/L at 20℃
[Hydrolytic Sensitivity]

8: reacts rapidly with moisture, water, protic solvents
[BRN ]

1794624
[LogP]

4.72 at 20℃
[CAS DataBase Reference]

10497-05-9(CAS DataBase Reference)
[EPA Substance Registry System]

Silanol, trimethyl-, phosphate (3:1) (10497-05-9)
Safety DataBack Directory
[Hazard Codes ]

F,Xi
[Risk Statements ]

R11:Highly Flammable.
R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S16:Keep away from sources of ignition-No smoking .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[RIDADR ]

UN 1993 3/PG 2
[WGK Germany ]

2
[RTECS ]

TC9700000
[F ]

10-21
[TSCA ]

Yes
[HS Code ]

2931.90.9010
[HazardClass ]

3.2
[PackingGroup ]

III
Hazard InformationBack Directory
[Chemical Properties]

Colorless liquid
[Uses]

Tris(trimethylsilyl) phosphite (TMSPi) is a film-forming additive for high voltage cathode material in lithium-ion batteries. Tris (trimethylsilyl) phosphate is cleaved by alkali-metal fluorides, nitrates, and acetates at give the trimethylsilyl esters of the corresponding acids.
[Definition]

ChEBI: Tris(trimethylsilyl) phosphate is an organosilicon compound that is phosphoric acid in which the three hydroxy groups are substituted by (trimethylsilyl)oxy groups. It is a phosphoric acid derivative and an organosilicon compound.
[Preparation]

Tris(trimethylsilyl)phosphine is prepared by treating trimethylsilyl chloride, white phosphorus, and sodium-potassium alloy:
1/4 P4 + 3 Me3SiCl + 3 K → P(SiMe3)3 + 3 KCl
[General Description]

Tris(trimethylsilyl) phosphate has been investigated as a novel film-forming additive for LiNi0.5Co0.2Mn0.3O2 cycling at high cut-off potential in LiPF6-based electrolyte. Tris(trimethylsilyl) phosphate [Tris(trimethylsilyl) ester of phosphoric acid] undergoes dealkylsilylation reaction with alumazene to yield heteroadamantane molecule.
[Reactivity Profile]

Tris(trimethylsilyl)phosphine and its more reactive derivative lithium bis-(trimethylsilyl)phosphide·2tetrahydrofuran are very useful reagents for the preparation of compounds with a single or a multiple element phosphorus bond. They react readily with various element halides, with carboxylic acid chlorides, and with carboxylic esters, as well as with other organic electrophiles via a substitution of lithium and/or a cleavage of the weak polar Si-P bonds.
[Flammability and Explosibility]

Notclassified
Spectrum DetailBack Directory
[Spectrum Detail]

Tris(trimethylsilyl)phosphate(10497-05-9)MS
Tris(trimethylsilyl)phosphate(10497-05-9)1HNMR
Tris(trimethylsilyl)phosphate(10497-05-9)13CNMR
Tris(trimethylsilyl)phosphate(10497-05-9)IR1
Tris(trimethylsilyl)phosphate(10497-05-9)Raman
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

10497-05-9(sigmaaldrich)
[TCI AMERICA]

Tris(trimethylsilyl) Phosphate,>98.0%(GC)(10497-05-9)
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