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ChemicalBook--->CAS DataBase List--->2373-51-5

2373-51-5

2373-51-5 Structure

2373-51-5 Structure
IdentificationMore
[Name]

CHLOROMETHYL METHYL SULFIDE
[CAS]

2373-51-5
[Synonyms]

CHLORODIMETHYL SULFIDE
CHLOROMETHYL METHYL SULFIDE
CHLOROMETHYL METHYL SULPHIDE
alpha-Chlorodimethyl sulfide
alpha-chlorodimethylsulfide
CH3SCH2Cl
Chloro(methylsulfanyl)methane
chloro(methylthio)-methan
chloro(methylthio)methane
Chlorodimethyl thioether
chlorodimethylthioether
Chloromethyl methyl thioether
chloromethylmethylthioether
Clorodimetilsolfuro
Methane, chloro(methylthio)-
Methylthiomethyl chloride
methylthiomethylchloride
Monochlorodimethyl sulfide
monochlorodimethylsulfide
Sulfide, chloromethyl methyl
[EINECS(EC#)]

219-148-4
[Molecular Formula]

C2H5ClS
[MDL Number]

MFCD00000923
[Molecular Weight]

96.58
[MOL File]

2373-51-5.mol
Chemical PropertiesBack Directory
[Appearance]

CLEAR YELLOW TO BROWN LIQUID
[Boiling point ]

105 °C (lit.)
[density ]

1.153 g/mL at 25 °C(lit.)
[refractive index ]

n20/D 1.498(lit.)
[Fp ]

63 °F
[storage temp. ]

2-8°C
[Water Solubility ]

Soluble in acetonitrile, ether and dichloromethane. Insoluble in water.
[Sensitive ]

Moisture Sensitive
[BRN ]

1730851
[CAS DataBase Reference]

2373-51-5(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

F,Xi
[Risk Statements ]

R11:Highly Flammable.
R37:Irritating to the respiratory system.
[Safety Statements ]

S9:Keep container in a well-ventilated place .
S16:Keep away from sources of ignition-No smoking .
S33:Take precautionary measures against static discharges .
[RIDADR ]

UN 1993 3/PG 2
[WGK Germany ]

3
[RTECS ]

WQ3700000
[F ]

13
[HazardClass ]

3
[PackingGroup ]

II
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Pentane-->Dimethyl sulfide-->Disiloxane, 1,1,1,3-tetraethoxy-3,3-dimethyl- (9CI)-->2-(Methylsulfinyl)acetophenone-->Chloromethyldichloromethylsilane-->Ethyldichlorosilane-->1,5-DICHLOROHEXAMETHYLTRISILOXANE-->1,3-DICHLORO-1,3-DIMETHYL-1,3-DIPHENYLDISILOXANE-->1,3-DICHLOROTETRAMETHYLDISILOXANE-->S-Methyl methanethiolsulfonate-->Bis(methylthio)methane-->Trichlorovinylsilane-->Hexamethylcyclotrisiloxane-->Decamethylcyclopentasiloxane-->Octamethylcyclotetrasiloxane
Hazard InformationBack Directory
[Chemical Properties]

CLEAR YELLOW TO BROWN LIQUID
[Uses]

Methylthiomethylating reagent for carbonyl and aromatic compounds. Methylene transfer reagent for iron(II) mediated cyclopropanation.
[Uses]

Chloromethyl methyl sulfide is used as a methylene transfer reagent for iron(II) mediated cyclopropanation and for carbonyl and aromatic compounds. It protects alcohols as their methylthiomethyl (MTM) ethers by reaction, e.g. with NaH/NaI in DME. It is also used for the preparation of MTM esters of carboxylic acids, e.g. by treatment of the K salt of the acid in the presence of NaI and 18-crown-6 and for reaction with cyclopentadienyl iron dicarbonyl dimer in the formation of an iron-containing methylene transfer agent.
[Synthesis Reference(s)]

Tetrahedron Letters, 35, p. 6127, 1994 DOI: 10.1016/0040-4039(94)88094-8
Spectrum DetailBack Directory
[Spectrum Detail]

CHLOROMETHYL METHYL SULFIDE(2373-51-5)MS
CHLOROMETHYL METHYL SULFIDE(2373-51-5)1HNMR
CHLOROMETHYL METHYL SULFIDE(2373-51-5)13CNMR
CHLOROMETHYL METHYL SULFIDE(2373-51-5)IR1
CHLOROMETHYL METHYL SULFIDE(2373-51-5)Raman
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

Chloromethyl methyl sulfide, 95%(2373-51-5)
[Sigma Aldrich]

2373-51-5(sigmaaldrich)
[TCI AMERICA]

Chloromethyl Methyl Sulfide,>97.0%(GC)(2373-51-5)
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