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ChemicalBook CAS DataBase List TRIETHYLENE GLYCOL MONOMETHYL ETHER
112-35-6

TRIETHYLENE GLYCOL MONOMETHYL ETHER synthesis

10synthesis methods
-

Yield:13826-35-2 87%

Steps:

1 EXAMPLE 1

The analysis indicated that the conversion of m-hydroxybenzyl alcohol was 99%, the yield of m-phenoxybenzyl alcohol was 93%, and the residue percentage of triethylene glycol monomethyl ether was 98% relative to the charged amount. The combined solution was also subjected to vacuum distillation, and there were recovered chlorobenzene and 162.5 g (purity: 98%, recovery: 97%) of triethylene glycol monomethyl ether, and there was obtained 71.6 g purity: 98%, isolation yield: 87%) of pure m-phenoxybenzyl alcohol.

References:

US5068459,1991,A

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