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ChemicalBook CAS DataBase List Stigmasterol
83-48-7

Stigmasterol synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 83 percent / propionic acid / xylene / Heating
2: 97 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
3: 277 mg / pyridine / 2 h / Ambient temperature
4: 187 mg / LiAlH4 / tetrahydrofuran / 2 h / Ambient temperature
5: p-TsOH*H2O / dioxane; H2O / 3 h / Heating

References:

Fujimoto, Yoshinori;Kimura, Miki;Khalifa, Fathy A. M.;Ikekawa, Nobuo [Chemical and pharmaceutical bulletin,1984,vol. 32,# 11,p. 4372 - 4381]

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