SALICYLIC ACID N-PROPYL ESTER synthesis
- Product Name:SALICYLIC ACID N-PROPYL ESTER
- CAS Number:607-90-9
- Molecular formula:C10H12O3
- Molecular Weight:180.2
71-23-8
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$12.00/100g
69-72-7
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$5.00/10g
607-90-9
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$45.00/2.5g
Yield: 96%
Reaction Conditions:
with alumina methanesulfonic acid at 120; for 0.333333 h;Microwave irradiation;
Steps:
Representative Procedure for Preparation of Aromatic and Aliphatic Esters (Table 1)
General procedure: In a typical reaction, AMA 2:3 (332 g, 0.6 mol), the corresponding carboxylicacid (1 mol), and alcohol (1.5-2 mol) were mixed in the provided reaction glass tubeequipped with a screw cap and magnetic agitation until a wet mixture was achieved.The reaction mixture was irradiated with microwaves (Anton Parr Monowave 300reactor) at 80 C for 8 min or 120 C for 20 min. On cooling, the mixture was diluted with dichloromethane (41 mL), filtered under gravity, and washed with dichloromethane;then the filtrate was washed with Na2CO3 (ss) and water. The organic layerwas dried over Na2SO4, filtered, and concentrated under reduced pressure to give theester.
References:
Fabian, Lucas;Gomez, Matias;Kuran, Juan A. Caturelli;Moltrasio, Graciela;Moglioni, Albertina [Synthetic Communications,2014,vol. 44,# 16,p. 2386 - 2392]
540-54-5
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69-72-7
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$5.00/10g
607-90-9
75 suppliers
$45.00/2.5g
71-23-8
757 suppliers
$12.00/100g
119-36-8
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607-90-9
75 suppliers
$45.00/2.5g
71-23-8
757 suppliers
$12.00/100g
56-23-5
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108-95-2
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94-13-3
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607-90-9
75 suppliers
$45.00/2.5g
