(R)-3-(Boc-Amino)piperidine synthesis
- Product Name:(R)-3-(Boc-Amino)piperidine
- CAS Number:309956-78-3
- Molecular formula:C10H20N2O2
- Molecular Weight:200.28
454713-13-4
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$27.00/100mg
309956-78-3
557 suppliers
$11.00/5g
Yield:309956-78-3 97%
Reaction Conditions:
with 5%-palladium/activated carbon;hydrogen in ethanol at 20 - 25; under 150015 Torr; for 20 h;
Steps:
6 Example 6: Synthesis of R-3-(tert-butoxycarbonylamino)piperidine (7)
R-3-(tert-butoxycarbonylamino)-1-benzylpiperidine (20g) was dissolved in 96g of absolute ethanol, added with 5 mass% Pd/C (2g), passed into 20MPa hydrogen, and reacted at 20-25 °C. After 20 h, filtration and ethanol washing, the filtrate was combined and evaporated to dryness to give R-3-(tert-butoxycarbonylamino)piperidine (13.4 g), yield 97%.
References:
CN110078657,2019,A Location in patent:Paragraph 0135-0136
485820-12-0
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309956-78-3
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![Carbamic acid, [(3R)-2-oxo-3-piperidinyl]-, 1,1-dimethylethyl ester (9CI)](/CAS/GIF/221874-51-7.gif)
221874-51-7
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$33.00/100mg
309956-78-3
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24424-99-5
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$13.50/25G
309956-78-3
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16682-12-5
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$9.00/1g
309956-78-3
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