Neopentylamine synthesis
- Product Name:Neopentylamine
- CAS Number:5813-64-9
- Molecular formula:C5H13N
- Molecular Weight:87.16
637-91-2
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5813-64-9
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Yield:-
Reaction Conditions:
with hydrogen in tetrahydrofuran at 140; under 30003 Torr; for 2.25 h;
Steps:
2 Effect of the Steric Requirement on the Selectivity of the Hydrogenation of Oximes
A mixture of 7.5 g of the oxime according to table 1, 175 ml of THF and 750 mg of Raney nickel were charged into a 200 ml pressure reactor and 40 bar of hydrogen were introduced under pressure at 140° C. After 135 min, the reactor was cooled to room temperature and depressurized. Raney nickel was filtered off and the filtrate was analyzed by gas chromatography. The results are summarized in table 1.
References:
US2013/66112,2013,A1 Location in patent:Paragraph 0093
630-18-2
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5813-64-9
161 suppliers
$17.00/1ml
![(E)-(2,2-dimethylpropylidene)({1-[(Z)-(2,2-dimethylpropylidene)amino]-2,2-dimethylpropyl})amine](/CAS/20200401/GIF/104410-32-4.gif)
75-84-3
257 suppliers
$10.00/1g
5813-64-9
161 suppliers
$17.00/1ml