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ChemicalBook CAS DataBase List N4-Acetylcytidine
3768-18-1

N4-Acetylcytidine synthesis

4synthesis methods
-

Yield:3768-18-1 96%

Reaction Conditions:

in acetonitrile; for 3 h;Reflux;

Steps:

1 Example 1: Preparation of Compound 4 Example

In a 500 mL three-necked flask was added 50.0 g of Compound 3 powder and 250 mL of acetonitrile and 25 mL of acetic anhydride, stirred and refluxed for 3 h, cooled to room temperature and filtered with suction. The solid was washed with acetonitrile twice and the filter cake was dried to give 56.3 g of compound 4 with a yield of 96.0 %.

References:

CN107033205,2017,A Location in patent:Paragraph 0033; 0034; 0035; 0036

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