ChemicalBook CAS DataBase List Methallyl acetate

Methallyl acetate synthesis

10synthesis methods

Product Name:Methallyl acetate
CAS Number:820-71-3
Molecular formula:C6H10O2
Molecular Weight:114.14

Methallyl acetate is produced from isobutene, acetic acid, and oxygen.

127-09-3 Synthesis

127-09-3
1075 suppliers
$8.00/1 ea

563-47-3
252 suppliers
$10.00/5g

820-71-3
99 suppliers
$13.00/1g

513-42-8
6 suppliers
$12.90/1g

Yield:820-71-3 92% ，513-42-8 5.5%

Reaction Conditions:

with sodium D-gluconate;copper(II) sulfate in water for 4 h;Reflux;Reagent/catalyst;

Steps:

3-4 Example 3
In the reaction kettle, add 2000 g of methallyl chloride, add 1800 g of sodium acetate, add 500 g of water, and add 60 g of copper sulfate. 800g, 20percent sodium gluconate aqueous solution was added dropwise, and the reaction temperature was controlled at reflux. After 4 hours of reaction, gas phase detection showed that the reaction was basically over. The content of each component was 0.5percent of raw material methallyl chloride, 92percent of methallyl acetate, 5.5percent of methallyl alcohol, and methallyl ether. 0.3percent.

References:

Ningbo Institute of Technology, Zhejiang University;Zhang Huaxing;Yang Zhijie;Lv Haixia;Jiang Yongjun CN111170828, 2020, A Location in patent:Paragraph 0026-0029

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