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ChemicalBook CAS DataBase List m-PEG8-Tos
79622-11-0

m-PEG8-Tos synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere
1.2: 20 °C / pH 3 / Inert atmosphere
2.1: sodium hydroxide / tetrahydrofuran; water / 0.17 h
2.2: 0 - 20 °C

References:

Liu, Xin;Yuan, Yaping;Bo, Shaowei;Li, Yu;Yang, Zhigang;Zhou, Xin;Chen, Shizhen;Jiang, Zhong-Xing [European Journal of Organic Chemistry,2017,vol. 2017,# 30,p. 4461 - 4468]

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