L-PHENYL-D5-ALANINE-2,3,3-D3 synthesis

3synthesis methods

Product Name:L-PHENYL-D5-ALANINE-2,3,3-D3
CAS Number:17942-32-4
Molecular formula:C9H3D8NO2
Molecular Weight:173.24

1-Imidazolidine-5-d-carboxylic acid, 2-(1,1-dimethylethyl)-3-methyl-4-oxo-5-(phenyl-d5-methyl-d2)-, 1,1-dimethylethyl ester, (2R-cis)- (9CI)

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17942-32-4
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Yield:-

Reaction Conditions:

with hydrogenchloride;Dowex 50-WX₈;acetic acid;trifluoroacetic acid1.) CH₂Cl₂, 30 min, 0 deg C; 12 h, room temperature; 2.) 100-105 deg C, toluene, water, 81 h;Yield given. Multistep reaction;

References:

Seebach, Dieter;Dziadulewicz, Edward;Behrendt, Linda;Cantoreggi, Sergio;Fitzi, Robert [Liebigs Annalen der Chemie,1989,p. 1215 - 1232]

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17942-32-4
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References

1-Imidazolidinecarboxylic acid, 2-(1,1-dimethylethyl)-3-methyl-4-oxo-5-(phenyl-d5-methyl-d2)-, 1,1-dimethylethyl ester, (2S-trans)- (9CI)

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17942-32-4
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References

L-PHENYL-D5-ALANINE-2,3,3-D3 Related Search:

L-Phenylalanine ETHYLBENZENE-2,3,4,5,6-D5 DL-PHENYLALANINE-2-D1 HYDROCINNAMIC-D5 ACID L-ALANINE-2-D1