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ChemicalBook CAS DataBase List L-Fucose
2438-80-4

L-Fucose synthesis

3synthesis methods
-

Yield:2438-80-4 66%

Reaction Conditions:

in water;isopropyl alcohol;

Steps:

8 Preparation of polymer 23

Preparation of polymer 23 Monomer 22 (460 mg, 1.44 mmol) and acrylamide (511 mg, 7.21 mmol) were dissolved in 4 mL of pure water and the solution was purged with nitrogen. Then, 5 mg of V-50 initiator was added and the solution was heated to 60° C. The solution became viscous within 30 minutes and heating was stopped. After 24 h, the viscous solution was added to isopropanol dropwise. The polymer was precipitated as a white mass which was filtered and dried in vacuum at room temperature for 48 h. The polymer was obtained as a white solid (640 mg) in 66% yield.

References:

US5891862,1999,A

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