Ethyl 4-amino-1-piperidinecarboxylate synthesis
- Product Name:Ethyl 4-amino-1-piperidinecarboxylate
- CAS Number:58859-46-4
- Molecular formula:C8H16N2O2
- Molecular Weight:172.22
29976-53-2
385 suppliers
$5.00/5g
58859-46-4
218 suppliers
$13.00/5g
Yield: 93%
Reaction Conditions:
Stage #1:N-ethoxycarbonyl-4-piperidone with titanium(IV) isopropylate;ammonia in ethanol at 25; for 6 h;
Stage #2: with sodium tetrahydroborate in ethanol at 25; for 3 h;Further stages.;
References:
Miriyala, Bruhaspathy;Bhattacharyya, Sukanta;Williamson, John S. [Tetrahedron,2004,vol. 60,# 7,p. 1463 - 1471]