DSIP synthesis
- Product Name:DSIP
- CAS Number:62568-57-4
- Molecular formula:C35H48N10O15
- Molecular Weight:848.82
4530-20-5
544 suppliers
$5.00/5G
35661-39-3
519 suppliers
$5.00/1g
71989-33-8
435 suppliers
$6.00/5g
71989-14-5
444 suppliers
$5.00/1g
71989-18-9
429 suppliers
$7.00/5g
![N-[(tert-Butoxy)carbonyl]-L-tryptophan](/CAS/GIF/13139-14-5.gif)
13139-14-5
359 suppliers
$8.00/10g
62568-57-4
246 suppliers
$34.50/1mg
Yield:-
Reaction Conditions:
Stage #1: Fmoc-Glu(OtBu)-OHwith methanol;N-ethyl-N,N-diisopropylamine in chloroform at 20; for 2 h;
Stage #2: with 4-methylpiperidin in chloroform;N,N-dimethyl-formamide;
Stage #3: BOC-glycine;N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine;Fmoc-Ser(tBu)-OH;Fmoc-(tBu)Asp-OH;Boc-Trp-OHFurther stages;
References:
Mikhaleva;Ivanov;Onoprienko;Prudchenko;Chikin;Yakubovskaya;Nemtsova;Bezborodova [Russian Journal of Bioorganic Chemistry,2014,vol. 40,# 1,p. 1 - 8][Bioorg. Khim.,2014,vol. 40,# 1,p. 3 - 11,9]