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ChemicalBook CAS DataBase List Cyclopropyl iodide
19451-11-7

Cyclopropyl iodide synthesis

3synthesis methods
4333-56-6 Synthesis
Cyclopropyl bromide

4333-56-6
380 suppliers
$6.00/5g

-

Yield:19451-11-7 64%

Reaction Conditions:

Stage #1:cyclopropyl bromide with lithium in diethyl ether at 0 - 20;Inert atmosphere;Schlenk technique;Glovebox;
Stage #2: with iodine in diethyl ether at -78 - 20;Inert atmosphere;Schlenk technique;

References:

Koch, Alexander;Dufrois, Quentin;Wirgenings, Marino;G?rls, Helmar;Krieck, Sven;Etienne, Michel;Pohnert, Georg;Westerhausen, Matthias [Chemistry - A European Journal,2018,vol. 24,# 63,p. 16840 - 16850]

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