ChemicalBook CAS DataBase List Benzimidazole

Benzimidazole synthesis

12synthesis methods

Product Name:Benzimidazole
CAS Number:51-17-2
Molecular formula:C7H6N2
Molecular Weight:118.14

50-00-0 Synthesis

50-00-0
864 suppliers
$10.00/25g

95-54-5 Synthesis

95-54-5
512 suppliers
$9.00/1g

51-17-2
576 suppliers
$14.00/25g

Yield:51-17-2 93%

Reaction Conditions:

with zinc oxide nanoparticle in ethanol at 25; for 0.166667 h;Sonication;Green chemistry;

Steps:

2.4. Synthesis of 2-benzimidazoles derivatives using ZnO NPs as catalyst
General procedure: In a typical procedure, aldehyde (10 mmol) and o-phenylenediamine(10 mmol) was dissolved in 10 ml ethanol. To this 0.5 mol% of ZnO (4.1 mg) nanocatalyst was added to the solution. The mixture was sonicated at a room temperature (25 °C) with ultrasound irradiation for 10 min. After completion of the reaction as indicated by the TLC, the reaction mixture was poured in ice cold water. The solid was filtered and the product was washed with water twice, dried and then purified by recrystallization from ethanol

References:

Paul, Bappi;Vadivel, Sethumathavan;Dhar, Siddhartha Sankar;Debbarma, Shyama;Kumaravel [Journal of Physics and Chemistry of Solids,2017,vol. 104,p. 152 - 159]

934-32-7 Synthesis