5-methoxy-1-[(4-methylphenyl)sulfonyl]-1H-Indole synthesis
- Product Name:5-methoxy-1-[(4-methylphenyl)sulfonyl]-1H-Indole
- CAS Number:139717-71-8
- Molecular formula:C16H15NO3S
- Molecular Weight:301.36
402822-76-8
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139717-71-8
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Yield:139717-71-8 100%
Reaction Conditions:
Stage #1: N-allyl-N-p-toluenesulfonyl-2-ethenyl-4-methoxyanilinewith trimethylsiloxyethene;tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride in dichloromethane; for 1.5 h;Heating;
Stage #2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride in benzene; for 3 h;Heating;
References:
Arisawa, Mitsuhiro;Terada, Yukiyoshi;Takahashi, Kazuyuki;Nakagawa, Masako;Nishida, Atsushi [Journal of Organic Chemistry,2006,vol. 71,# 11,p. 4255 - 4261]
139717-69-4
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139717-71-8
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139717-79-6
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139717-71-8
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