5-Methoxyindole
- CAS No.
- 1006-94-6
- Chemical Name:
- 5-Methoxyindole
- Synonyms
- 5-METHOXY-1H-INDOLE;Methoxyindole 99% indol-5-yl methyl ether;5-methoxy-indol;Femedol;NSC 521752;AKOS JY2082918;5-METHOXYINDOLE;methoxy-5indole;5-MethoxyindoleF;Methoxy-5 indole
- CBNumber:
- CB4223553
- Molecular Formula:
- C9H9NO
- Molecular Weight:
- 147.17
- MDL Number:
- MFCD00005674
- MOL File:
- 1006-94-6.mol
- MSDS File:
- SDS
Melting point | 52-55 °C (lit.) |
---|---|
Boiling point | 176-178 °C/17 mmHg (lit.) |
Density | 1.1135 (rough estimate) |
refractive index | 1.5310 (estimate) |
Flash point | 176-178°C/17mm |
storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
solubility | Chloroform, Methanol |
form | Crystalline Powder |
pka | 16.70±0.30(Predicted) |
color | White to light brownish |
Water Solubility | insoluble |
Sensitive | Light Sensitive |
BRN | 116722 |
InChIKey | DWAQDRSOVMLGRQ-UHFFFAOYSA-N |
CAS DataBase Reference | 1006-94-6(CAS DataBase Reference) |
EWG's Food Scores | 1 |
FDA UNII | DQM3AS43PQ |
NIST Chemistry Reference | 1H-Indole, 5-methoxy-(1006-94-6) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H315-H319-H335 | |||||||||
Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 | |||||||||
Hazard Codes | Xi | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 26-36-24/25-37/39 | |||||||||
WGK Germany | 3 | |||||||||
RTECS | NL9500000 | |||||||||
F | 8 | |||||||||
Hazard Note | Irritant | |||||||||
HazardClass | IRRITANT, KEEP COLD, LIGHT SENSITIVE | |||||||||
HS Code | 29339900 | |||||||||
NFPA 704 |
|
5-Methoxyindole price More Price(31)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich | M14900 | 5-Methoxyindole 99% | 1006-94-6 | 1g | $26 | 2024-03-01 | Buy |
Sigma-Aldrich | M14900 | 5-Methoxyindole 99% | 1006-94-6 | 5g | $35.4 | 2024-03-01 | Buy |
TCI Chemical | M0731 | 5-Methoxyindole >99.0%(GC) | 1006-94-6 | 1g | $42 | 2024-03-01 | Buy |
TCI Chemical | M0731 | 5-Methoxyindole >99.0%(GC) | 1006-94-6 | 5g | $72 | 2024-03-01 | Buy |
Alfa Aesar | B25290 | 5-Methoxyindole, 99% | 1006-94-6 | 1g | $36.65 | 2024-03-01 | Buy |
5-Methoxyindole Chemical Properties,Uses,Production
Chemical Properties
white to light brownish crystalline powder
Uses
5-Methoxyindole (cas# 1006-94-6) is a compound useful in organic synthesis. It can be used to synthesis 1-(Phenylsulfonyl)-5-methoxy-1H-indole.
Definition
ChEBI: 5-methoxyindole is a member of indoles.
Preparation
The synthesis of 5-methoxyindole from 5-methoxy-2-oxindole: Conversion of 5-methoxy-2-oxindole to 5-methoxyindole was accomplishedby the chlorination of 5-methoxy-2-oxindole with triphenylphosphine-carbontetrachloride in acetonitrile followed by the catalytic reduction of a chlorine atom in 66% total yield.
Reactions
5-methoxyindole was treated with sodium hydroxide and phenylsulfonyl chloride in the presence of a catalytic amount of tetrabutylammonium bromide to afford 1-(phenylsulfonyl)indole and 5-methoxy-1-(phenylsufonyl)indole in excellent yields of 100%.
Synthesis Reference(s)
Journal of Heterocyclic Chemistry, 26, p. 1405, 1989 DOI: 10.1002/jhet.5570260533
The Journal of Organic Chemistry, 58, p. 5558, 1993 DOI: 10.1021/jo00072a052
Tetrahedron Letters, 27, p. 837, 1986 DOI: 10.1016/S0040-4039(00)84114-3
Purification Methods
Crystallise 5-methoxyindole from cyclohexane pet ether or pet ether/Et2O. [Saito & Kikugawa J Heterocycl Chem 16 1325 1979, Beilstein 21 III/IV 765, 21/3 V 18.]
5-Methoxyindole Preparation Products And Raw materials
Raw materials
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Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Shanghai UCHEM Inc. | +862156762820 +86-13564624040 | sales@myuchem.com | China | 7562 | 58 |
Hebei Chuanghai Biotechnology Co,.LTD | +86-13131129325 | sales1@chuanghaibio.com | China | 5890 | 58 |
Capot Chemical Co.,Ltd. | +86-(0)57185586718 +86-13336195806 | sales@capot.com | China | 29791 | 60 |
Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | info@tianfuchem.com | China | 21634 | 55 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32957 | 60 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29881 | 58 |
Zhejiang ZETian Fine Chemicals Co. LTD | +8618957127338 | stella@zetchem.com | China | 2136 | 58 |
Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10311 | 58 |
Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28172 | 58 |
Hebei Weibang Biotechnology Co., Ltd | +8615531157085 | abby@weibangbio.com | China | 8810 | 58 |
View Lastest Price from 5-Methoxyindole manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2024-11-05 | 5-Methoxyindole
1006-94-6
|
US $0.00-0.00 / KG | 5mg | 99%HPLC | 2000tons | Shaanxi Dideu Medichem Co. Ltd | ||
2024-11-01 | 5-Methoxyindole
1006-94-6
|
US $129.00-645.00 / g | 1g | 0.99 | 25kg | Shanghai UCHEM Inc. | ||
2024-10-11 | 5-Methoxyindole
1006-94-6
|
US $11.00 / ASSAYS | 1ASSAYS | 99% | 10000kg | Hebei Chuanghai Biotechnology Co,.LTD |
- 5-Methoxyindole
1006-94-6
- US $0.00-0.00 / KG
- 99%HPLC
- Shaanxi Dideu Medichem Co. Ltd
- 5-Methoxyindole
1006-94-6
- US $129.00-645.00 / g
- 0.99
- Shanghai UCHEM Inc.
- 5-Methoxyindole
1006-94-6
- US $11.00 / ASSAYS
- 99%
- Hebei Chuanghai Biotechnology Co,.LTD
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