4-Morpholinoaniline synthesis
- Product Name:4-Morpholinoaniline
- CAS Number:2524-67-6
- Molecular formula:C10H14N2O
- Molecular Weight:178.23
10389-51-2
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$15.00/5g
2524-67-6
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$8.00/1g
Yield:2524-67-6 99%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in ethanol at 20; for 3 h;
Steps:
5.1.62. 1-methyl-1H-pyrazol-4-amine (18a)
General procedure: To 17a (1 g, 7.8 mmol) in EtOH (20 mL) was added 10% Pd/C50 mg. The reaction mixture was stirred for 3 h under hydrogen at roomtemperature. The mixture was then filtered with Celite, and the filtratewas concentrated and dried under vacuum to yield 0.74 g (97%) of 18aas a white solid. MS (ESI) m/z 98 [M+H]+.
References:
Yu, Ru-Nan;Chen, Cheng-Juan;Shu, Lei;Yin, Yuan;Wang, Zhi-Jian;Zhang, Tian-Tai;Zhang, Da-Yong [Bioorganic and Medicinal Chemistry,2019,vol. 27,# 8,p. 1646 - 1657]
70291-67-7
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$21.00/1g
2524-67-6
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$8.00/1g
30483-75-1
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$6.00/1g
2524-67-6
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$8.00/1g
350-46-9
516 suppliers
$10.60/1gm:
2524-67-6
302 suppliers
$8.00/1g