4-Cyanobenzoyl chloride synthesis
- Product Name:4-Cyanobenzoyl chloride
- CAS Number:6068-72-0
- Molecular formula:C8H4ClNO
- Molecular Weight:165.58
619-65-8
360 suppliers
$9.00/1g
6068-72-0
234 suppliers
$17.67/250mgs:
Yield:6068-72-0 98%
Steps:
62 Example 62
After dry nitrogen gas was introduced to the reaction mixture for one hour, acetonitrile was removed under ambient pressure, and was further removed under reduced pressure through distillation, to thereby obtain 16.2 g of p-cyanobenzoyl chloride (yield 98%, based on p-cyanobenzoic acid). The p-cyanobenzoyl chloride obtained had a purity of 99%.
References:
Showa Denko Kabushiki Kaisha US6433211, 2002, B1
1877-72-1
283 suppliers
$7.00/5g
6068-72-0
234 suppliers
$17.67/250mgs:
1711-11-1
111 suppliers
$17.00/250mg
3058-39-7
274 suppliers
$10.00/1g
122-04-3
8 suppliers
$15.00/1g
636-98-6
24 suppliers
$17.00/5g
6068-72-0
234 suppliers
$17.67/250mgs:
105-07-7
395 suppliers
$5.00/5g
6068-72-0
234 suppliers
$17.67/250mgs: