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ChemicalBook CAS DataBase List 4-CYANO-2'-NITRODIPHENYL
75898-34-9

4-CYANO-2'-NITRODIPHENYL synthesis

10synthesis methods
-

Yield:75898-34-9 96%

Reaction Conditions:

Stage #1: ortho-nitrobenzoic acidwith potassium carbonate in various solvent(s) at 120; for 0.5 h;
Stage #2: 4-Cyanochlorobenzenewith 1,10-Phenanthroline;copper(l) iodide in various solvent(s) at 160; for 24 h;Further stages.;

References:

Goossen, Lukas J.;Rodriguez, Nuria;Melzer, Bettina;Linder, Christophe;Deng, Guojun;Levy, Laura M. [Journal of the American Chemical Society,2007,vol. 129,# 15,p. 4824 - 4833]

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