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ChemicalBook CAS DataBase List 2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester
34874-90-3

2,4-Dihydroxy-3-formyl-6-methylbenzoic acid methyl ester synthesis

9synthesis methods
-

Yield:34874-90-3 87%

Reaction Conditions:

Stage #1: methyl orsellinatewith titanium tetrachloride in dichloromethane at 0; for 0.166667 h;Inert atmosphere;
Stage #2: Dichloromethyl methyl ether in dichloromethane at 0 - 20; for 1 h;Inert atmosphere;

References:

Dong, Chunmao;Huo, Luqiong;Liu, Hongxin;Lu, Xiuxiang;Qiu, Shengxiang;Tan, Haibo;Wang, Miaomiao;Yang, Bao;Yuan, Yunfei;Zhang, Wenge [Organic Letters,2020] Location in patent:supporting information

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