ChemicalBook CAS DataBase List 3,5-Diiodo-L-tyrosine dihydrate

3,5-Diiodo-L-tyrosine dihydrate synthesis

4synthesis methods

Product Name:3,5-Diiodo-L-tyrosine dihydrate
CAS Number:300-39-0
Molecular formula:C9H9I2NO3
Molecular Weight:432.98

Diiodotyrosine, 3,5-diiodotyrosine (25.2.1), is synthesized by directly iodinating tyrosine with iodine in the presence of sodium iodide in aqueous ethylamine, or in a mixture of acetic and hydrochloric acids with the addition of hydrogen peroxide.

60-18-4 Synthesis

60-18-4
843 suppliers
$15.00/25g

300-39-0
271 suppliers
$10.00/5g

Yield:300-39-0 84.63%

Reaction Conditions:

with hydrogen iodide;acetic acid in dimethyl sulfoxide at 65; for 0.025 h;

References:

Puratchikody, Ayarivan;Umamaheswari, Appavoo;Irfan, Navabshan;Sinha, Shweta;Manju;Ramanan, Meera;Ramamoorthy, Gayathri;Doble, Mukesh [New Journal of Chemistry,2019,vol. 43,# 2,p. 834 - 846] Location in patent:supporting information

FullText

60-18-4 Synthesis

60-18-4
843 suppliers
$15.00/25g

300-39-0
271 suppliers
$10.00/5g

70-78-0 Synthesis