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ChemicalBook CAS DataBase List 3',5'-di-o-p-chlorobenzoyl-2-deoxy-5-azacytosine
1034301-08-0

3',5'-di-o-p-chlorobenzoyl-2-deoxy-5-azacytosine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: hydrogenchloride / 0 - 20 °C
2: triethylamine / acetone / 10 h / 20 - 55 °C
3: trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 5 h / 20 - 85 °C

References:

Shanghai Lark Pharmaceutical Technology Co., Ltd.;Hu Xiaochuan;Yang Jidong;Shen Xin;Li Feng;Wang Jian;Hou Qian;Dong Qin CN110028537, 2019, A

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