ChemicalBook CAS DataBase List 2,6-Dibromo-4-methylaniline

2,6-Dibromo-4-methylaniline synthesis

12synthesis methods

Product Name:2,6-Dibromo-4-methylaniline
CAS Number:6968-24-7
Molecular formula:C7H7Br2N
Molecular Weight:264.95

106-49-0
397 suppliers
$5.00/5 g

583-68-6 Synthesis

583-68-6
291 suppliers
$10.00/5 g

6968-24-7
210 suppliers
$10.00/5g

Yield:6968-24-7 75% ，583-68-6 20%

Reaction Conditions:

with N-Bromosuccinimide in chloroform at 20; for 0.5 h;Temperature;Solvent;

Steps:

General procedure for the preparation of compounds 1a-6c and 7
General procedure: p-Toluidine (1.07 g, 0.01 mol) or 4-[(phenylsulfonyl)amino]toluene (2.77 g, 0.01 mol) wasdissolved in CHCl3 and stirred for 5 min at RT. Nbromosuccinimide(NBS) (3.56 g, 0.02 mol) wasadded, and the reaction mixture was stirred for 0.5 hr.After filtration, the filtrate was concentrated, and themixture was purified by column chromatography.

References:

Fang, Lei;Zhang, Haun;Fang, Xubin;Gou, Shaohua;Cheng, Lin [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2014,vol. 53,# 5,p. 635 - 641]

106-49-0
397 suppliers
$5.00/5 g

6968-24-7
210 suppliers
$10.00/5g

References