5-CHLORO-1,3-DIHYDRO-2H-PYRROLO[3,2-B] PYRIDIN-2-ONE synthesis

2synthesis methods

Product Name:5-CHLORO-1,3-DIHYDRO-2H-PYRROLO[3,2-B] PYRIDIN-2-ONE
CAS Number:136888-08-9
Molecular formula:C7H5ClN2O
Molecular Weight:168.58

16013-85-7 Synthesis

16013-85-7
486 suppliers
$9.00/5g

5-CHLORO-1,3-DIHYDRO-2H-PYRROLO[3,2-B] PYRIDIN-2-ONE

136888-08-9
93 suppliers
$177.47/250mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sodium hydride / 1,2-dimethoxyethane / 2 h / 20 °C
1.2: 18 h / 20 °C
2.1: hydrogen / ethanol; water / 48 h / 2280.15 Torr
2.2: 5 h / Reflux

References:

Hoffmann-La Roche Inc.;Alam, Muzaffar;Du Bois, Daisy Jo;Hawley, Ronald Charles;Minatti, Ana Elena;Kennedy-Smith, Joshua;Thakkar, Kshitij Chhabilbhai;Wilhelm, Robert Stephen US2013/158066, 2013, A1

16013-85-7 Synthesis

16013-85-7
486 suppliers
$9.00/5g

105-53-3
755 suppliers
$5.00/25g

136888-08-9
93 suppliers
$177.47/250mg

References

5-CHLORO-1,3-DIHYDRO-2H-PYRROLO[3,2-B] PYRIDIN-2-ONE Related Search:

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