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ChemicalBook CAS DataBase List 1-Methylcyclopentanol
1462-03-9

1-Methylcyclopentanol synthesis

9synthesis methods
-

Yield:1462-03-9 39%

Reaction Conditions:

with water;Amberlyst 15 in isopropyl alcohol at 55;

Steps:

B.9
B) Hydration of 1-methylcyclopentene Examples 6-9In a continuously operated glass reactor (internal diameter 25 mm; height 200 mm), an ion exchanger (Amberlyst type) was introduced as catalyst. In trickle mode, at a constant internal volume, the mixture consisting of 1-methylcyclopentene, isopropanol (iPrOH) and water was introduced from a storage container via a membrane pump.The product mixture was analyzed by GC. The yields and conversions were calculated from GC % by weight results.

References:

BASF SE US2012/101306, 2012, A1 Location in patent:Page/Page column 6

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