1-METHOXY-2-BUTANOL synthesis
- Product Name:1-METHOXY-2-BUTANOL
- CAS Number:53778-73-7
- Molecular formula:C5H12O2
- Molecular Weight:104.15
106-88-7
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15467-25-1
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53778-73-7
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Yield: 38% ， 58%
Reaction Conditions:
with graphite oxide at 20; for 1 h;
Steps:
General procedure for the alcoholysis of epoxides:
General procedure: To a solution of epoxide(1 mmol) and alcohol (5 mmol) was added 1 mg of graphite oxide (GO) at room temperature and the mixture stirred for the time indicated in Table 2 prior to GC/MS analysis. CH2Cl2 was added and the mixture was filtered and evaporated under reduced pressure. Pure products were isolated by flash column chromatography using hexane/EtOAc (6:1) as eluent.
References:
Mirza-Aghayan, Maryam;Alizadeh, Mahdi;Molaee Tavana, Mahdieh;Boukherroub, Rabah [Tetrahedron Letters,2014,vol. 55,# 49,p. 6694 - 6697]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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53778-73-7
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106-88-7
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$15.00/25mL
124-41-4
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53778-73-7
46 suppliers
$15.00/1g
106-88-7
159 suppliers
$15.00/25mL
67-56-1
746 suppliers
$7.29/5ml-f
53778-73-7
46 suppliers
$15.00/1g
