1-Acetyl-2-imidazolidinone synthesis
- Product Name:1-Acetyl-2-imidazolidinone
- CAS Number:5391-39-9
- Molecular formula:C5H8N2O2
- Molecular Weight:128.13
120-93-4
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5391-39-9
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Yield:5391-39-9 64.1%
Reaction Conditions:
at 150; for 1 h;
Steps:
10
5.18 g (60.2 mmol) of 2-imidazolidone and 50 mL of acetic anhydride were added to a 100 mL recovery flask, and the mixture was stirred at an oil bath temperature of 150 ° C. for 1 hour. After cooling to room temperature, the precipitated solid was collected by filtration and washed with a small amount of cold ethanol to obtain 4.94 g (yield: 64.1%) of colorless solid 1-acetyl-2-imidazolidone.
References:
TOSOH CORPORATION;SAGAMI CHEMICAL RESEARCH INSTITUTE;AKIYAMA, EIICHI;KAMOHARA, TAKAO;KONDO, SATOSHI;IMATOMI, SHINYA;YAMADA, SATORU JP2016/145198, 2016, A Location in patent:Paragraph 0087-0089
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120-93-4
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5391-39-9
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1001-53-2
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5391-39-9
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