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ChemicalBook CAS DataBase List [1,2-ethanediylbis(oxy-2,1-ethanediyloxy)]-bis-
32775-08-9

[1,2-ethanediylbis(oxy-2,1-ethanediyloxy)]-bis- synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 48 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) room temp., 2 h
2: 97 percent / CF3COOH / CH2Cl2 / 1 h / Ambient temperature

References:

Wittmann, Valentin;Takayama, Shuichi;Gong, Ke Wei;Weitz-Schmidt, Gabriele;Wong, Chi-Huey [Journal of Organic Chemistry,1998,vol. 63,# 15,p. 5137 - 5143]

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