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ChemicalBook CAS DataBase List 1,2,3,5-Tetrafluorobenzene
2367-82-0

1,2,3,5-Tetrafluorobenzene synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: H2SiEt2; tetrabutylammonium triphenyldifluorosilicate / benzene-d6; tetrahydrofuran / 40 h / 80 °C / Inert atmosphere; Sealed tube
2: H2SiEt2; tetrabutylammonium triphenyldifluorosilicate / benzene-d6; tetrahydrofuran / 40 h / 60 °C / Inert atmosphere; Sealed tube

References:

Kikushima, Kotaro;Grellier, Mary;Ohashi, Masato;Ogoshi, Sensuke [Angewandte Chemie - International Edition,2017,vol. 56,# 51,p. 16191 - 16196][Angew. Chem.,2017,vol. 129,p. 16409 - 16414,6]

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